Preparation method of heat-resisting solid solution blue and white porcelain
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A technology of solid solution, blue and white porcelain, applied in the field of heat-resistant solid solution blue and white porcelain preparation, can solve the problems of cracking of glaze layer, failure to meet the quality requirements of blue and white porcelain, cracking of green body, etc., and achieves the effect of avoiding high temperature oxidation, low cost and improving quality
Inactive Publication Date: 2014-08-06
ANHUI QINGHUAFANG FINE BONE PORCELAIN
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Problems solved by technology
For ordinary blue and white porcelain, when the fired products are heated during use, the thermal expansion coefficients of the body and the glaze are inconsistent, which will cause the glaze layer to crack, and in severe cases, the body will crack together.
It cannot meet the quality requirements of modern consumers for blue and white porcelain
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[0015] The temperature in the heating step is controlled at 1000-1400°C.
[0016] The general formula of the solid solution is: a(Bi x K 1-x ) TiO 3 –bBiFeO 3 , where a+b=1, a is in the range of 0.50-0.55, and x is in the range of 0.01-0.50.
[0017] specific:
[0018] The 1-bromo-3-methyl-2-butene is 0.08-0.09% by weight.
[0019] The 3-ethoxy-4-carboxybenzyl is 0.04-1% by weight.
[0020] The 0.04-1.50% holmium trifluoroacetylacetonate is 0.08-0.11% by weight.
[0021] The above are the embodiments of the present invention, so all equivalent changes or modifications made according to the structure, features and principles described in the scope of the application of the present invention are included in the scope of the patent application of the present invention.
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Abstract
The invention discloses a preparation method of heat-resisting solid solution blue and white porcelain, which mainly comprises the steps of raising temperature, drying, sintering, keeping warm, cooling, taking out from a kiln, and the like. The heat-resisting solid solution blue and white porcelain comprises the following components in percentage by weight: 20-65 percent of silicon dioxide, 0.01-1 percent of hydroquinone, 0.01-1 percent of zinc oxide, 0.05-2 percent of ammonium heptamolybdate, 0.01-2 percent of ethyl acetate, 15-35 percent of aluminium oxide, 0.1-3 percent of ferric oxide, 0.04-1.50 percent of trifluoroacetylacetone holmium, 5 to 10 percent of calcium oxide, 5-10 percent of magnesium oxide, 3-6 percent of potassium oxide, 1-5 percent of sodium oxide, 1-10 percent of lithium oxide, 0.01-2 percent of rutile type titanium dioxide, 0.06-2 percent of 1-bromine-3-methyl-2-butene and 0.01-1.55 percent of 3-ethyoxyl-4- carboxyl benzyl. According to the invention, the problem of high temperature oxidization during a firing process can be avoided in a better manner; a finished product is high in heat-resistant performance, and piezoelectric behavior can be shown; zero pollution can be caused, and the cost is low.
Description
technical field [0001] The invention relates to a preparation method of blue-and-white porcelain, in particular to a preparation method of heat-resistant solid solution blue-and-white porcelain. Background technique [0002] Blue and white porcelain (blue and white porcelain), often referred to as blue and white, is one of the mainstream varieties of Chinese porcelain. Blue and white is painted and decorated on white clay with natural cobalt, then covered with transparent glaze, and then fired at a high temperature of 1300 degrees Celsius, so that the color material can fully penetrate into the glaze, showing green and blue patterns. It looks quiet and beautiful, clean and elegant. For ordinary blue and white porcelain, when the fired products are heated during use, the thermal expansion coefficients of the body and the glaze are inconsistent, which will cause the glaze layer to crack, and in severe cases, the body will crack together. It cannot meet the quality requiremen...
Claims
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