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A method for improving the magnetic properties of sintered NdFeB thin slice magnets

A technology of neodymium iron boron and magnetic properties, applied in the direction of magnetic materials, magnetic objects, inorganic materials, etc., can solve problems such as difficult to realize industrialization, achieve high uniformity of distribution and thickness consistency, and improve the coercive force of magnetic sheets , Improve the effect of tissue structure and composition

Active Publication Date: 2017-03-01
NINGBO YUNSHENG +2
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, due to the limitations of the physical properties of sintered NdFeB thin-film magnets, the preparation technology of the suspension and the heat treatment technology, it is still difficult to apply the spraying technology to the grain boundary diffusion technology to obtain distribution uniformity and thickness on the surface of the sintered NdFeB thin-film magnets. Coating with high consistency and grain boundary diffusion technology is difficult to achieve industrialization when improving the magnetic properties of sintered NdFeB thin-film magnets

Method used

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  • A method for improving the magnetic properties of sintered NdFeB thin slice magnets
  • A method for improving the magnetic properties of sintered NdFeB thin slice magnets
  • A method for improving the magnetic properties of sintered NdFeB thin slice magnets

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Embodiment 1

[0024] Embodiment 1: A method for improving the magnetic properties of sintered NdFeB thin-plate magnets, comprising the following steps:

[0025] ① Preparation of heavy rare earth compound powder, the heavy rare earth compound is DyF3, and the particle size of the powder is ≤10 μm;

[0026] ② Disperse the heavy rare earth compound powder in absolute ethanol, mix well to obtain a suspension, and the viscosity of absolute ethanol at normal temperature and pressure is 1.08mpa.s.

[0027] ③Spray the suspension evenly on the surface of the sintered NdFeB thin sheet magnet to form a coating, and the sintered NdFeB thin sheet magnet has been surface pretreated before spraying;

[0028] ④ Dry the sprayed sintered NdFeB thin-slice magnets. The drying process is to keep warm at 80 ° C for 1 hour, and the dried sintered NdFeB thin-slice magnets are stored in an inert gas environment;

[0029] ⑤ Put the dried sintered NdFeB thin sheet magnet at a pressure of 1×10 -4 In the inert gas en...

Embodiment 2

[0038] Embodiment 2: A method for improving the magnetic properties of sintered NdFeB flake magnets, comprising the following steps:

[0039] ① Preparation of heavy rare earth compound powder, the heavy rare earth compound is DyF3, and the particle size of the powder is ≤10 μm;

[0040] ② Disperse the heavy rare earth compound powder in a mixed solvent with a viscosity of about 4.0mpa.s at room temperature and pressure obtained by mixing absolute ethanol and ethylene glycol, and stir evenly to obtain a suspension.

[0041] ③Spray the suspension evenly on the surface of the sintered NdFeB thin sheet magnet to form a coating, and the sintered NdFeB thin sheet magnet has been surface pretreated before spraying;

[0042] ④ Dry the sprayed sintered NdFeB thin-slice magnets. The drying process is to keep warm at 120 ° C for 1 hour, and the dried sintered NdFeB thin-slice magnets are stored in an inert gas environment;

[0043] ⑤ Put the dried sintered NdFeB thin sheet magnet at a p...

Embodiment 3

[0049] Embodiment three: a method for improving the magnetic performance of a sintered NdFeB thin slice magnet, comprising the following steps:

[0050] ① Preparation of heavy rare earth compound powder, the heavy rare earth compound is DyF3, and the particle size of the powder is ≤10 μm;

[0051] ② Disperse the heavy rare earth compound powder in the pva solution prepared by 1788 type polyvinyl alcohol and water. The mass percentage of 1788 type polyvinyl alcohol is 7%. The viscosity under normal pressure is 26mpa.s.

[0052] ③Spray the suspension evenly on the surface of the sintered NdFeB thin sheet magnet to form a coating, and the sintered NdFeB thin sheet magnet has been surface pretreated before spraying;

[0053] ④ Dry the sprayed sintered NdFeB thin-slice magnets. The drying process is to keep warm at 120 ° C for 1 hour, and the dried sintered NdFeB thin-slice magnets are stored in an inert gas environment;

[0054] ⑤ Put the dried sintered NdFeB thin sheet magnet a...

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Abstract

The invention discloses a method for improving the magnetic property of sintered NdFeB flaky magnets. First, suspension liquid containing heavy rare earth elements and having the viscosity of 0.1 to 500 mpa.s in the conditions of normal temperature and pressure is sprayed onto the surface of a sintered NdFeB flaky magnet uniformly. Second, the sintered NdFeB flaky magnet is dried, and then a coating containing heavy rare earth elements is obtained on the surface of the sintered NdFeB flaky magnet. Finally, the diffusion treatment and the ageing treatment are carried out on the dried sintered NdFeB flaky magnet in the environment of inert gas. The method has the advantages that the spraying technology can be applied to the grain boundary diffusion technique successfully, more specifically, a coating with high distribution uniformity and thickness distribution can be obtained on the surface of sintered NdFeB flaky magnets, and the grain boundary diffusion technology can be applied industrially for improving the magnetic property of sintered NdFeB flaky magnets.

Description

technical field [0001] The invention relates to a processing method for a sintered NdFeB thin-slice magnet, in particular to a method for improving the magnetic properties of a sintered NdFeB thin-slice magnet. Background technique [0002] With the significant progress of science and technology and rapid economic development, the demand for sintered NdFeB materials used in many fields such as scientific research, industry, household appliances and office automation is increasing. High-performance sintered NdFeB materials are used in computers , Precision machine tools, detectors, measuring instruments, automotive motors and various permanent magnet motors have a wide range of application backgrounds. At the same time, with the accelerated development of "low-carbon economy", the promotion speed and application range of sintered NdFeB materials in high-end fields such as wind power, inverter compressors, and hybrid power have expanded rapidly. At the same time, in recent ye...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01F41/02H01F1/057H01F1/08C23C10/28
Inventor 竺晓东曾许多吕向科丁勇张民石高阳
Owner NINGBO YUNSHENG