Two-component adhesive layer polyurethane resin for synthetic leather and preparation method of two-component adhesive layer polyurethane resin
A polyurethane resin and two-component technology, applied in the direction of polyurea/polyurethane adhesives, adhesive types, adhesives, etc., to achieve the effect of increasing turnover times and utilization efficiency, and reducing production energy consumption
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Embodiment 1
[0019] The raw materials used in this embodiment and their weight are shown in Table 1.
[0020] Table 1
[0021] raw material name
Weight (unit: g)
Polytetrahydrofuran ether glycol (number average molecular weight 2000)
320
32.16
Ethylene glycol
14.88
diphenylmethane diisocyanate
144
125.25
83.5
[0022] The preparation steps of the two-component adhesive layer polyurethane resin for synthetic leather of the present embodiment are as follows:
[0023] 1) Put 104g of dimethylformamide, 320g of polytetrahydrofuran ether glycol, 32.16g of 2,2-dimethylolpropionic acid and 14.88g of ethylene glycol into the reaction kettle, and stir evenly at 50-55°C;
[0024] 2) Put 144g of diphenylmethane diisocyanate into the reactor in batches, strictly control the reaction temperature between 65-70°C, and react under normal pressure for 7 hours, and u...
Embodiment 2
[0026] The raw materials used in this embodiment and their weight are shown in Table 2.
[0027] Table 2
[0028] raw material name
Weight (unit: g)
Polybutylene adipate diol (number average molecular weight 1000)
40
Polybutylene adipate diol (number average molecular weight 3000)
120
6.432
[0029] Ethylene glycol
11.904
diphenylmethane diisocyanate
80
506
126.5
[0030] The preparation steps of the two-component adhesive layer polyurethane resin for synthetic leather of the present embodiment are as follows:
[0031] 1) Mix 190g of dimethylformamide, 40g of polybutylene adipate diol with a number average molecular weight of 1000, 120g of polybutylene adipate diol with a number average molecular weight of 3000, 6.432g2,2 - Put dimethylolpropionic acid and 11.904g ethylene glycol into the reaction kettle, and stir...
Embodiment 3
[0034] The raw materials used in this embodiment and their weight are shown in Table 3.
[0035] table 3
[0036]
[0037] The preparation steps of the two-component adhesive layer polyurethane resin for synthetic leather of the present embodiment are as follows:
[0038] 1) Mix 171g of dimethylformamide, 320g of polyethylene adipate, butanediol copolyester diol, 5.36g of 2,2-dimethylolpropionic acid, 1.8g of 1,4-butanediol and 1.24g of ethyl Put the diol into the reaction kettle, stir evenly at 55-60°C;
[0039] 2) Put 60g of diphenylmethane diisocyanate into the reaction kettle in batches, strictly control the reaction temperature between 75-80°C, and react at normal pressure for 9 hours, and according to the viscosity of the system, use the remaining dimethylformamide and butyl The ketone is diluted in stages, and the final viscosity is controlled at 60-120Pa.S25°C to obtain a two-component adhesive layer polyurethane resin for synthetic leather.
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