Lithium ion battery diaphragm for overcharge protection and preparation method thereof
A lithium-ion battery, overcharge protection technology, applied in secondary batteries, battery pack components, circuits, etc., to achieve the effects of good effect, easy mass production, and simple and controllable preparation method
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[0078] Example 1:
[0079] Fluorencarbazole copolymer and triphenylamine-fluorene copolymer, polyvinylidene fluoride-copolymer-hexafluoropropylene (PVDF-HFP), polyethylene oxide (PEO) and tin oxide are mixed in a mass ratio of 1:0.5:0.1 , The mass ratio of fluorencarbazole copolymer and triphenylamine-fluorene copolymer is 9:1, and the mass ratio of PVDF-HFP and PEO is 5:1; then it is dissolved in chloroform and N,N-dimethylformamide (DMF), stir uniformly at a speed of 1300 rpm, and then heat to a temperature of 80°C and continue to stir until it is completely dissolved to obtain a mixture; the obtained mixture is electrostatically charged at a voltage of 25 kV and a receiving distance of 20 cm. After spinning, the product was collected by a flat current collector after 2 hours, then separated, formed into holes, and dried in a vacuum oven at 80°C for 12 hours to obtain a lithium ion battery separator with a thickness of 50 μm.
[0080] Structure diagram such as figure 2 Shown.
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Example Embodiment
[0084] Example 2:
[0085] Mix fluorenebenzene copolymer, triphenylamine-fluorene copolymer, polyvinylidene fluoride-copolymer-hexafluoropropylene (PVDF-HFP), polyacrylonitrile (PAN), and salicylic acid in a mass ratio of 1:8:0.5 , Wherein the mass ratio of fluorenebenzene copolymer and triphenylamine-fluorene copolymer is 1:5, the mass ratio of PVDF-HFP and PAN is 7:3; then it is dissolved in tetrachloromethane, N,N-dimethylethyl In amide (DMAc) and N,N-dimethylformamide (DMF), stir uniformly at a speed of 500 rpm, and then heat to a temperature of 60 ℃ and continue to stir until completely dissolved to obtain a mixture; Under the conditions of voltage of 5kV and receiving distance of 7cm, electrospinning, after 2 hours, collect the product with a flat current collector, then remove 85% by mass of the inactive components inside the product, and then separate, form holes, It was dried in a vacuum oven at 60°C for 14 hours to obtain a lithium ion battery separator with a thicknes...
Example Embodiment
[0088] Example 3
[0089] Fluorencarbazole copolymer and fluorenebenzene copolymer, polyvinylidene fluoride-copolymer-hexafluoropropylene (PVDF-HFP), glycerin are weighed according to the mass ratio of 1:15:10, of which the fluorencarbazole copolymer and The mass ratio of the fluorenebenzene copolymer is 8:2; then the active polymer and the inactive polymer are separately dissolved in N,N-dimethylformamide (DMF), stirred evenly at a speed of 1300 rpm, and then heated Continue to stir until the temperature is 80℃ to completely dissolve to obtain two mixtures; place the obtained two mixtures in a concentric structure of the electrospinning needle tip, under the conditions of a voltage of 15kV and a receiving distance of 20cm, electrospinning for 1 hour Then, the product was collected by a solution-rotating current collector, and then separated, formed into holes, and dried in a vacuum oven at 90°C for 11 hours to obtain a lithium ion battery separator with a thickness of 50 μm.
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