Lithium-ion secondary battery
A secondary battery and lithium-ion technology, applied in secondary batteries, lithium batteries, battery electrodes, etc., can solve problems such as the performance impact of lithium-ion secondary batteries, and achieve excellent low-temperature characteristics and excellent cycle characteristics.
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Embodiment 1
[0268] (1-1. Manufacturing method of water-soluble polymer)
[0269] Add 32.5 parts of methacrylic acid (ethylenically unsaturated carboxylic acid monomer) and 2,2,2-trifluoroethyl methacrylate (fluorine-containing (meth)acrylate monomer) into a 5MPa pressure vessel with a stirrer. Body) 7.5 parts, ethylene glycol dimethacrylate (crosslinkable monomer) 0.8 parts, butyl acrylate (optional monomer) 58.0 parts, polyoxyalkylene alkenyl ether ammonium sulfate (reactive surface Active agent monomer, manufactured by Kao Corporation, trade name "LATEMUL PD-104") 1.2 parts, t-dodecyl mercaptan 0.6 parts, ion exchange water 150 parts, and potassium persulfate (polymerization initiator) 0.5 parts, sufficient To stir. Then, it was heated to 60°C to initiate polymerization. Cooling was performed when the polymerization conversion rate reached 96%, the reaction was stopped, and a mixture containing a water-soluble polymer was obtained. 10% ammonia water was added to the mixture containing t...
Embodiment 2
[0292] Except that in the above (1-1), the amount of 2,2,2-trifluoroethyl methacrylate was changed to 3 parts, and the amount of butyl acrylate was changed to 62.5 parts, the same as Example 1 A lithium ion secondary battery was manufactured and evaluated.
Embodiment 3
[0294] Except that in the above (1-1), the amount of 2,2,2-trifluoroethyl methacrylate was changed to 18 parts, and the amount of butyl acrylate was changed to 47.5 parts, the same as in Example 1 A lithium ion secondary battery was manufactured and evaluated.
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