Recyclable graphene

A graphene and graphite technology, applied in the field of graphene, can solve the problems of impurity removal, low stripping yield, difficulty in removing residual solvent, etc., and achieve the effect of simple process and good quality

Inactive Publication Date: 2014-12-24
QINGDAO JINXIU SHUIYUAN COMMERCE & TRADE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, studies have shown that the yield of graphene prepared by the solvent stripping method has a great relationship with the solvent. Generally, N-2-methylpyrrolidone (NMP), N,N-dimethylformamide (DMF) and other high-boiling-point ones are selected. Organic solvents, there is a problem that it is difficult to remove residual solvents
In addition, even if a suitable solvent is selected, the yield of simple solvent stripping is generally very low, further improving the stripping yield requires adding inorganic salts, alkalis or surfactants, etc., and there is also the problem of impurity removal.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0010] A kind of recyclable graphene, including the following parts by weight: 13 parts of graphite fluoride, 11 parts of hexabromine aqueous dispersion, 13 parts of methacryl cyclohexene, 10 parts of quartz sand, 15 parts of methanol , 75 parts of graphite, 5 parts of butyryl tri-n-hexyl citrate, 15 parts of nonylhexyl trimellitate, 1 part of fly ash, 50 parts of ethylene glycol benzoate, and 78 parts of water.

Embodiment 2

[0012] A kind of recyclable graphene, including the following parts by weight: 27 parts of fluorinated graphite, 23 parts of hexabromine aqueous dispersion, 28 parts of methacryl cyclohexene, 14 parts of quartz sand, 15 parts of methanol 36 parts, 80 parts of graphite, 8 parts of butyryl tri-n-hexyl citrate, 27 parts of nonylhexyl trimellitate, 5 parts of fly ash, 77 parts of ethylene glycol benzoate, and 80 parts of water.

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PUM

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Abstract

The invention discloses recyclable graphene which comprises the following substances in parts by weight: 13-27 parts of carbon monofluoride, 11-23 parts of a hexa-bromine water dispersed body, 13-28 parts of methyl allyl cyclohexene, 10-14 parts of quartz sand, 15-36 parts of methanol, 75-80 parts of graphite, 5-8 parts of butyryltrihexylcitrate, 15-27 parts of nonyl hexyl trimellitate, 1-5 parts of coal ash, 50-77 parts of diethylene glycol benzoate and 78-80 parts of water. The process is simple and can be performed in multiple polar solvents, and the obtained graphene is good in quality and can be recycled when being used as graphene quantum dots for auxiliary peeling.

Description

technical field [0001] The present invention relates to a kind of recyclable graphene. Background technique [0002] Graphene is a nano-carbon material with a hexagonal lattice honeycomb structure formed by sp2 hybridization of a single layer of carbon atoms, which belongs to a new type of two-dimensional crystal material. Graphene has good electrical conductivity, thermal conductivity, optical transparency, and special mechanical and electronic properties. It has good application prospects in energy storage, transparent conductive devices, composite materials, and optoelectronic devices. Therefore, graphene has become a research hotspot in many disciplines such as materials science, physics and chemistry. [0003] The preparation methods of graphene mainly include mechanical exfoliation method, chemical vapor deposition method, oxidation intercalation re-reduction method and liquid phase exfoliation method. Among them, both mechanical exfoliation and chemical vapor deposi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/04
Inventor 王省业
Owner QINGDAO JINXIU SHUIYUAN COMMERCE & TRADE
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