Method for absorbing microwaves by adopting dielectric/ferromagnetic composite material
A composite material and dielectric technology, applied in radiation-absorbing coatings, chemical instruments and methods, and other chemical processes, etc., can solve problems such as narrow absorption frequency bands, and achieve the effect of wide frequency band, broad application prospects, and low density.
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Embodiment 1
[0023] Described dielectric / ferromagnetic composite microwave absorbing material, its preparation steps are:
[0024] (1) Using the sol-gel method, using ethylene glycol methyl ether and monoethanolamine as solvents, lanthanum nitrate and nickel acetate as starting materials, and annealing in air at 700 ° C for 1.5 hours to obtain a loose and porous nickel acid with oxygen vacancies Lanthanum powder (as figure 1 shown);
[0025] (2) Carbon-coated iron-cobalt nanocapsules were prepared by DC plasma arc method;
[0026] (3) 50wt% lanthanum nickelate (LaNiO 3 ) powder and 50wt% carbon-coated iron-cobalt (FeCo / C) nanocapsules are dispersed in ethanol, and then the two suspensions are ultrasonically mixed, mixed evenly and then dried to obtain LaNiO 3 - FeCo / C (50 / 50) composite material.
[0027] (4) Preparation of absorbing samples:
[0028] 0.4g LaNiO prepared in step (3) 3 - FeCo / C (50 / 50) composite material mixed with 0.6g paraffin (LaNiO 3 -FeCo / C (50 / 50) composite mate...
Embodiment 2
[0030] Described dielectric / ferromagnetic composite microwave absorbing material, its preparation steps are:
[0031] (1) Using the sol-gel method, using ethylene glycol methyl ether and monoethanolamine as solvents, lanthanum nitrate and nickel acetate as starting materials, and annealing in air at 700 ° C for 1.5 hours to obtain a loose and porous nickel acid with oxygen vacancies Lanthanum powder (as figure 1 shown);
[0032] (2) Carbon-coated iron-cobalt nanocapsules were prepared by DC plasma arc method;
[0033] (3) 80wt% lanthanum nickelate (LaNiO 3 ) powder and 20wt% carbon-coated iron-cobalt (FeCo / C) nanocapsules are dispersed in ethanol, and then the two suspensions are ultrasonically mixed, mixed evenly and then dried to obtain LaNiO 3 - FeCo / C (80 / 20) composite material.
[0034] (4) Preparation of absorbing samples:
[0035] 0.4g LaNiO prepared in step (3) 3 - FeCo / C (80 / 20) composite material mixed with 0.6g paraffin (LaNiO 3 -FeCo / C (80 / 20) composite mate...
Embodiment 3
[0037] The difference from Example 2 is: lanthanum nickelate (LaNiO 3 ) powder and carbon-coated iron-cobalt (FeCo / C) nanocapsules with a mass ratio of 20:80, the resulting composite material is LaNiO 3 -FeCo / C(20 / 80), the reflection loss of the absorbing sample made of this composite material has an absorption lower than -10dB at different frequencies (see Figure 6 ).
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