Water-soluble benzotriazole imidazoline extreme-pressure anti-wear reagent and preparation method thereof
A technology for benzotriazole acetate imidazole and benzotriazole, which is applied in the field of benzotriazole imidazoline derivatives and their preparation, can solve problems such as poor oil solubility and water solubility, and achieves good extreme pressure, good Water-soluble, high-yield effect
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example 1
[0020] Example 1: Add 20g of benzotriazole to a 250ml three-neck flask, add 100ml of water as a solvent, add 8.0g of NaOH, stir and react at 90°C for 3 hours, and continuously add 18g of chlorine dropwise within half an hour Acetic acid aqueous solution, react at 90°C for 3 hours, cool the product at room temperature and add HCl until a large amount of white precipitates appear, filter and wash chloride ions, obtain 11.24g of benzotriazole acetic acid after drying, and then add two Toluene as a solvent and water carrier, 8ml of diethylenetriamine, react at 140-160°C for 4 hours to remove the water generated in the reaction, react at 190-210°C for 2 hours to remove the water generated in the reaction, and distill under reduced pressure to obtain light yellow Brown viscous liquid imidazolyl ethylamine benzotriazole acetate.
example 2
[0021] Example 2: Add 20g of benzotriazole to a 250ml three-necked flask, add 100ml of water as a solvent, add 8.0g of NaOH, stir and react at 90°C for 3 hours, and continuously dropwise add 18.0g of benzotriazole within half an hour Chloroacetic acid aqueous solution, react at 90°C for 3 hours, cool the product at room temperature and add HCl until a large amount of white precipitates appear, filter and wash chloride ions, obtain 11.09g of benzotriazole acetic acid after drying, and then add them to a 250ml three-necked flask Xylene as solvent and water carrier, 8ml of N-hydroxyethylethylenediamine, react at 140-160°C for 4h to remove the water generated in the reaction, react at 190-210°C for 2~3h to remove the water generated in the reaction, Distill under reduced pressure to obtain a light yellow-brown viscous liquid benzotriazole acetic acid imidazolyl ethanol.
example 3
[0022] Example 3: Add 20g of benzotriazole to a 250ml three-necked flask, add 100ml of water as a solvent, add 8.0g of NaOH, stir and react at 90°C for 3 hours, and continuously add 18.0g of benzotriazole dropwise within half an hour Chloroacetic acid aqueous solution, react at 90°C for 3 hours, cool the product at room temperature and add HCl until a large amount of white precipitates appear, filter and wash chloride ions, obtain 11.19g of benzotriazole acetic acid after drying, and then add them to a 250ml three-necked flask Xylene is used as solvent and water-carrying agent, 8.2ml of triethylenetetramine, react at 140-160°C for 4~6h to remove the water generated in the reaction, react at 190-210°C for 2~3h to remove the water generated in the reaction, reduce Pressure distillation, that is, light yellow brown viscous liquid benzotriazole acetic acid imidazolylethylaminoethylamine.
[0023] All target compounds were determined by Spectrum One infrared spectrometer to have im...
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