Composition containing acrylic acid (ester)/sodium acryloyl nitrogen copolymer as well as preparation and preparation method thereof
A technology of sodium acryloyl nitrogen copolymer and composition, which is applied in the field of surface chemistry to achieve the effects of good user experience, novel appearance and good spreadability
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Embodiment 1
[0075] Embodiment 1 Preparation of emulsifier-free composition
[0076]
[0077] 1. Pour raw material A into a dry water phase pot, stir evenly, add water, heat up to 80 degrees, and set aside;
[0078] 2. Pour B into a stainless steel bucket, stir well, and use a moving homogenizer to homogenize it, and set it aside;
[0079] 3. Heat the emulsification pot to 60 degrees, vacuumize, start stirring, first pump phase A, then pump phase B;
[0080] 4. Vacuum and homogenize for 3 minutes;
[0081] 5. Turn off homogenization, turn on stirring for 30 rpm, and at the same time turn on cooling water to cool down at a rate of one degree per minute;
[0082] 6. Continue to stir and cool down to 30 degrees;
[0083] 7. Filtration and discharge.
Embodiment 2
[0084] Embodiment 2 Emulsifier-free cream
[0085]
[0086]
[0087] See Example 1 for the preparation method.
Embodiment 3
[0088] Embodiment 3 Preparation of emulsifier-free sunscreen
[0089]
[0090] 1) Pour the other ingredients of A except water into a dry water phase pot, stir evenly, add water, heat up to 80 degrees, and set aside;
[0091] 2) Pour B into a stainless steel barrel, stir well and homogenize with a moving homogenizer, when the fineness of titanium dioxide reaches 40, pour into an oil phase pot, heat to 80 degrees, and set aside;
[0092] 3) Heat the emulsification pot to 60 degrees, vacuumize, start stirring, first pump phase A, then pump phase B;
[0093] 4) Vacuum and homogenize for 3 minutes;
[0094] 5) Turn off homogenization, turn on stirring for 30 rpm, and at the same time turn on cooling water to cool down at a rate of one degree per minute;
[0095] 6) When the temperature drops to 40 degrees, add C, continue to stir and cool down to 30 degrees;
[0096] 7) filter the discharge.
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