Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for improving filter-pressing performance of particles in poly-aluminum ferric chloride

A technology for polyaluminum ferric chloride and particulate matter, which is applied in chemical instruments and methods, iron halide, water/sewage treatment, etc., can solve the problems of slow reaction speed, small flocs of polyaluminum salt, and small residual color, and saves money. cost, improving the performance of particulate matter filter press, and the effect of good water treatment

Inactive Publication Date: 2015-04-08
CHANGZHOU UNIV
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, polymeric aluminum salts and polymeric iron salts have outstanding features but have their own shortcomings. Polymeric aluminum salts have small flocs, weak hydrolysis, and slow sedimentation. The treated water contains toxic substances, but the water treatment effect is good, and the residual color is small. Polymerized iron salts Strong hydrolysis, large flocs, good strength, but large residual chroma
This prompted the birth of polyaluminum ferric sulfate, but generally polyaluminum ferric sulfate is used in water treatment, and the reaction speed is slow

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0027] After the bauxite is carefully cleaned, dried, and preliminarily crushed, it is put into a horse-boiling furnace and calcined at 800°C for 3 hours, ground to 120 mesh, 200g of bauxite powder is put into a four-necked reaction bottle, and 50mL of lime water is added. Stir 20mL of calcium chloride hexahydrate for 20 minutes, add 60mL of 0.98 concentrated sulfuric acid to the stirred solution, reflux at 120-140°C for 4 hours, cool to room temperature, add 20g of coal powder and iron powder, and continue to reflux at 120°C for 30 minutes , stop heating, continue to stir for 30 minutes, add 20g polyacrylamide to the stirred polyaluminum ferric chloride, stir well, put it in the reaction kettle for 2 hours at 200°C, and age it for 24 hours to obtain deep red Brown liquid polyaluminum ferric chloride. Take 200mL of polluted waste water and put them into two reaction bottles respectively, add the above-mentioned flocculant and polyaluminum ferric chloride in the reaction bottle...

example 2

[0029] After the bauxite is carefully cleaned, dried, and preliminarily crushed, it is put into a horse-boiling furnace and calcined at 800°C for 3.5 hours, ground to 120 mesh, 200g of bauxite powder is put into a four-necked reaction bottle, and 50mL of lime water is added. Stir 20mL of calcium chloride hexahydrate for 20 minutes, add 60mL of 0.98 concentrated sulfuric acid to the stirred solution, reflux at 130°C for 4 hours, cool to room temperature, add 20g of coal powder and iron powder, continue to reflux at 120°C for 30 minutes, stop Heat and keep stirring for 35 minutes, add 20g of polyacrylamide to the stirred polyaluminum ferric chloride, stir well, put it in the reaction kettle for 2 hours at 210°C, and age for 24 hours to obtain a dark reddish-brown liquid polyaluminum ferric chloride. Take 200mL of polluted waste water and put them into two reaction bottles respectively, add the above-mentioned flocculant and polyaluminum ferric chloride in the reaction bottles re...

example 3

[0031] After the bauxite is carefully cleaned, dried, and preliminarily crushed, it is put into a horse-boiling furnace for calcination at 800°C for 4 hours, ground to 120 mesh, 200g of bauxite powder is put into a four-necked reaction bottle, and 50mL of lime water is added. Stir 20mL of calcium chloride hexahydrate for 20 minutes, add 60mL of 0.98 concentrated sulfuric acid to the stirred solution, reflux at 140°C for 4 hours, cool to room temperature, add 20g of coal powder and iron powder, continue to reflux at 140°C for 30 minutes, stop Heat and keep stirring for 40 minutes, add 20g of polyacrylamide to the stirred polyaluminum ferric chloride, stir well, put it in the reaction kettle for 2 hours at 220°C, and age for 24 hours to obtain a dark reddish-brown liquid polyaluminum ferric chloride. Take 200mL of polluted waste water and put them into two reaction bottles respectively, add the above-mentioned flocculant and polyaluminum ferric chloride in the reaction bottles r...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a method for improving filter-pressing performance of particles in poly-aluminum ferric chloride. The method is characterized by comprising the following steps: calcining bauxite at 800 DEG C for 3-4 hours, grinding and filtering by 120 meshes, adding lime water and calcium chloride hexahydrate, stirring for 20 minutes, adding concentrated sulfuric acid to a stirred solution, refluxing for 4 hours at 120-140 DEG C, cooling to room temperature, adding pulverized coal and iron powder, continuing to reflux for 30 minutes at 120-140 DEG C, stopping heating, continuing to stir for 30-40 minutes, adding polyacrylamide, fully stirring, reacting at 200-220 DEG C for 2 hours in a reaction kettle, and aging for 24 hours so as to obtain dark brown liquid poly-aluminum ferric chloride. The removal rate of the poly-aluminum ferric chloride after improving the filter-pressing performance of particles is 19.22% higher than that of others.

Description

technical field [0001] The invention relates to a method for improving the pressure filtration performance of particulate matter in polyaluminum ferric chloride. Background technique [0002] With the development of science and technology, many water treatment methods have emerged, such as ion exchange, biofilm, adsorption, chemical oxidation, point dialysis and flocculation. Among them, flocculation hair is the most widely used, with the strongest applicability, low cost and obvious treatment effect. The most widely used flocculants for flocculation and sedimentation are inorganic polymer flocculants, which mainly include polymeric aluminum salts and polymeric iron salts. However, polymeric aluminum salts and polymeric iron salts have outstanding features but have their own shortcomings. Polymeric aluminum salts have small flocs, weak hydrolysis, and slow sedimentation. The treated water contains toxic substances, but the water treatment effect is good, and the residual co...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/52C01G49/10
CPCC02F1/5236C01G49/10
Inventor 徐炜
Owner CHANGZHOU UNIV