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Composite manufacturing method of optical ultra-broadband anti-reflection coating

An anti-reflection film and ultra-broadband technology, applied in the field of broadband anti-reflection film preparation, can solve the problem that the anti-reflection performance needs to be improved, and achieve the effects of good hydrophobicity and self-cleaning performance, transmission bandwidth, and good environmental adaptability.

Inactive Publication Date: 2016-05-18
NANJING INST OF ASTRONOMICAL OPTICS & TECH NAT ASTRONOMICAL OBSE
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

But its anti-reflection performance needs to be improved

Method used

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  • Composite manufacturing method of optical ultra-broadband anti-reflection coating
  • Composite manufacturing method of optical ultra-broadband anti-reflection coating

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Embodiment 1

[0025] Embodiment 1, the preparation method of broadband anti-reflection coating. The anti-reflection film preparation process is as follows:

[0026] 1. Preparation: Clean the vacuum chamber, coating fixture, etc., put magnesium fluoride and aluminum oxide film materials in the electron gun crucible, clean the optical lenses, put them in the vacuum chamber and close the vacuum chamber door.

[0027] 2. Vacuuming and optical lens heating steps: Start the vacuum pump to evacuate and gradually raise the temperature to 300 degrees Celsius. The heating step and constant temperature time are determined according to the size and shape of the optical lens.

[0028] 3. Vacuum coating step: at a baking temperature of 300 degrees Celsius, the magnesium fluoride layer is evaporated first, and the thickness of the evaporated film layer is 83 nanometers, and then the aluminum oxide layer is evaporated at the same temperature. The film thickness is 4 nm.

[0029] 4. The film-forming step ...

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Abstract

A combination technology method for an ultra-wideband anti-reflection film includes the steps of vacuum evaporation film forming and sol-gel film forming. According to the technology of vacuum evaporation film forming, for preparation work, all related appliances inside a vacuum room are cleaned, an optical lens is placed into the vacuum room, and film materials are added; vacuumizing is performed; the film materials are preheated; the film materials are gasified and deposited on the surface of the optical lens; baking is performed for 60 minutes; magnesium fluoride layer evaporation is performed; aluminum oxide layer evaporation is performed at the same baking temperature, wherein the thickness of an evaporated film layer is 4 nanometers. The vacuum evaporation film forming technology is implemented from the step (1) to the step (6), and the sol-gel film forming technology is implemented from the step (7) to the step (10). The number of layers of the wideband anti-reflection film is decreased, and the bandwidth region of an existing wideband anti-reflection film is widened. Through a film plating after-treatment technology, the layers of the film have good hydrophobicity and self-cleaning performance, and good environment adaptability is achieved. By the adoption of the combination film forming method, the average transmittance within the waveband range of 300 nm-1000 nm can reach 98.5%.

Description

technical field [0001] The invention relates to the technical field of optical coating processing, in particular to a preparation method of a broadband antireflection film. Background technique [0002] Anti-reflection coated lens is an important optical device, and its application has penetrated into many fields of scientific instruments such as aerospace remote sensing, laser communication, photovoltaic cells, and ground-based telescopic instruments. From the analysis of structural design, the broadband anti-reflection coating lens is a combination of optical substrate and multi-layer dielectric film. In order to increase the transmission bandwidth, three kinds of high, medium and low refractive index materials are usually used to form a multi-layer film. The most commonly used is Al 2 o 3 —ZrO 2 —MgF 2 collocation, but this collocation structure is complex and can only cover a limited spectral bandwidth. [0003] Vacuum anti-reflection film coating process commonly u...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G02B1/115C23C14/24C23C14/08C23C14/06
CPCC23C14/0694C23C14/081C23C14/24C23C18/1254C23C28/04G02B1/115
Inventor 王晋峰王烨儒田杰
Owner NANJING INST OF ASTRONOMICAL OPTICS & TECH NAT ASTRONOMICAL OBSE