Preparation method for polyurethane adhesive applied to protective film
A polyurethane adhesive and protective film technology, applied in the direction of polyurea/polyurethane adhesives, adhesives, film/sheet adhesives, etc., can solve the problems of white fog, poor mechanical properties, poor heat resistance and oxidation resistance, etc. , to achieve the effect of low adhesion, good wetting performance and outstanding hydrolysis resistance
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Embodiment 1
[0027] A kind of preparation method of polyurethane adhesive for protective film, its steps are as follows:
[0028] (1) Prepolymerization reaction: Install a mechanical stirring bar, a thermometer, a condenser and a nitrogen gas inlet on a 250ml three-necked flask. Weigh 10.435g of polyether triol with a number average molecular weight of 4000, 30g of toluene, 4.489g of hexamethylene diisocyanate, and 0.002g of dibutyltin dilaurate, dissolve the polyether triol in toluene, stir well , add hexamethylene diisocyanate and dibutyltin dilaurate, under the condition of stirring, heat the three-necked flask in a water bath to 70°C and keep it for 4h for prepolymerization;
[0029] (2) Chain extension reaction: After the above prepolymerization reaction is complete, add a mixture of 35.3g of toluene and 50.377g of polycarbonate diol with a number average molecular weight of 500, and raise the temperature of the water bath to 90°C, keep it for 5h, and stop After reaction, a colorless...
Embodiment 2
[0034] (1) Prepolymerization reaction: Install a mechanical stirring bar, a thermometer, a condenser and a nitrogen gas inlet on a 250ml three-necked flask. Weigh 7.214g of polyether diol with a number average molecular weight of 3000, 30g of toluene, 4.489g of hexamethylene diisocyanate, 0.002g of stannous octoate, dissolve the polyether triol in toluene, stir well, add Hexamethylene diisocyanate and dibutyltin dilaurate, under stirring conditions, the three-necked flask was heated to 70°C in a water bath and kept for 4 hours for prepolymerization;
[0035] (2) Chain extension reaction: After the above prepolymerization reaction is complete, add a mixture of 35.3g of toluene and 50.377g of polycarbonate triol with a number average molecular weight of 3000, and raise the temperature of the water bath to 95°C, keep it for 4h, and stop After reaction, a colorless transparent liquid is obtained, which is polyurethane adhesive.
[0036] In this embodiment, the reaction raw materi...
Embodiment 3
[0039] (1) Prepolymerization reaction: Install a mechanical stirring bar, a thermometer, a condenser and a nitrogen gas inlet on a 250ml three-necked flask. Weigh 5.691g of polyether triol with a number average molecular weight of 500, 30g of toluene, 4.489g of hexamethylene diisocyanate, and 0.002g of dibutyltin diacetate, dissolve the polyether triol in toluene, stir well, Add hexamethylene diisocyanate and dibutyltin dilaurate, and under stirring conditions, the temperature of the water bath is raised to 80°C and kept for 2 hours for prepolymerization;
[0040] (2) Chain extension reaction: After the prepolymerization reaction is complete, add a mixture of 35.3 g of toluene and 54.949 g of polycarbonate diol with a number average molecular weight of 2000, and raise the temperature of the water bath to 85 ° C. After 6 hours of reaction, stop After reaction, a colorless transparent liquid is obtained, which is polyurethane adhesive.
[0041] In this embodiment, the reaction ...
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