Plastic expanding agent for settlement resistance of high flow state cement based cementing material and preparation method thereof
A technology of plastic expansion agent and cementitious material, applied in the field of plastic expansion agent and its preparation, high fluidity concrete/mortar, can solve the problems of unfavorable development of concrete strength and durability, fast reaction speed, large gas generation, etc. Improve the ability of slurry to resist segregation and bleeding, improve viscosity, and improve the effect of homogeneity
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[0030] First of all, the specific embodiment of the present invention is generally described: a plastic expansion agent for anti-settling of a high fluidity cement-based cementitious material, which is made of the following raw materials in weight percentage: azo compound, stabilizer, catalyst, Rheological additive; its formula ratio range is as follows:
[0031] Azo compounds: 30-50 parts;
[0032] Stabilizer: 10-30 parts;
[0033] Catalyst: 5-20 parts;
[0034] Rheology additive: 20-40 parts.
[0035] The azo compound is an aromatic organic macromolecule containing amine groups. Among them, the number of C atoms in organic macromolecules directly affects the anti-sedimentation and compensation shrinkage effects. According to the test results of fluidity and swelling capacity, it is preferred to use azo aromatic compounds with C atoms between 12 and 18 as the main raw materials, specifically p-aminoazobenzene, p-nitrobenzenediazoaminoazobenzene, 4-(diethylamino)azobenzene,...
Embodiment 1
[0043] p-aminoazobenzene: 15 parts;
[0044] p-Nitrobenzenediazoaminoazobenzene: 20 parts;
[0045] Glyceryl stearate: 25 parts;
[0046] Potassium carbonate: 5 parts;
[0047] Sodium silicate: 7 parts;
[0048] Organic bentonite: 28 parts.
[0049] The plastic expansion agent for anti-settling of high-flow cement-based cementitious materials prepared according to the above ratio is mixed into C40 concrete at 0.2‰ of the cementitious materials in ordinary concrete. The early plastic shrinkage rate of the concrete is 0%, the 28-day free expansion rate reaches 0.12%, and the 28-day compressive strength is increased by 3% compared with the benchmark concrete.
Embodiment 2
[0051] 4,4'-Azophenetyl oxide: 20 parts;
[0052] p-aminoazobenzene: 20 parts;
[0053] Tripolyglycerol monostearate: 20 parts;
[0054] Polyethylene glycol stearate: 10 parts;
[0055] Potassium hydroxide: 3 parts;
[0056] Sodium bicarbonate: 5 parts;
[0057] Organic bentonite: 17 parts;
[0058] Modified hydrogenated castor oil: 5 parts.
[0059] The plastic expansion agent for anti-settling of high-flow cement-based cementitious materials prepared according to the above ratio is mixed into C30 concrete at 0.2‰ of the cementitious materials in ordinary concrete. The early plastic shrinkage rate of the concrete is 0.05%, the 28-day free expansion rate reaches 0.1%, and the 28-day compressive strength is increased by 2% compared with the benchmark concrete.
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