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Method for extracting bergamot fruit essential oil through continuous phase transition at low temperature and bergamot fruit essential oil

A low-temperature continuous phase change, bergamot technology, applied in the direction of essential oils/spice, fat production, etc., can solve the problems of low temperature continuous phase change extraction, no reference regularity, etc., to achieve continuity suitable for large-scale industrialization The effect of production, reducing the loss of low-boiling point components, and convenient operation

Active Publication Date: 2015-08-05
SOUTH CHINA AGRI UNIV +1
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  • Claims
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Problems solved by technology

The low-temperature continuous phase change extraction process conditions summarized in existing studies are usually related to the key factors such as the particle size of raw materials, extraction temperature, pressure and time, but not only that, the process conditions are also closely related to the types of raw materials, for different There is no regularity that can be referred to between the technical solutions, and the fine adjustment of key factors will have a huge impact on the final effect of the low-temperature continuous phase-change extraction. Using low-temperature continuous phase-change extraction of bergamot The study of aroma components such as volatile oil has not been reported

Method used

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  • Method for extracting bergamot fruit essential oil through continuous phase transition at low temperature and bergamot fruit essential oil
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  • Method for extracting bergamot fruit essential oil through continuous phase transition at low temperature and bergamot fruit essential oil

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Embodiment 1

[0024] Embodiment 1 bergamot low temperature continuous phase change extraction process research experiment

[0025] According to the characteristics of the bergamot raw materials, the present invention continuously analyzes and determines and adjusts the process conditions. Follow the steps below:

[0026] S1. Bergamot (derived from Guangdong Zhancui Food Co., Ltd.) was crushed to an appropriate mesh size, dried at 50°C to make the moisture ≤ 13%, and bergamot powder was obtained;

[0027] S1. Weigh the bergamot powder obtained in S1 according to the bulk density requirements of different raw materials and put it directly into the extraction tank 1, pressurized by the high-pressure pump 7 to make the n-butane pass through the heat exchanger 8I, and enter the extraction tank 1 to determine its The extraction is carried out at the extraction temperature and pressure, and the solvent through the extraction tank 1 enters the analysis tank 2I with oil, where it is analyzed, and t...

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Abstract

The invention discloses a method for extracting bergamot fruit essential oil through continuous phase transition at a low temperature. The method comprises the following steps: crushing bergamot fruits until the granularity is 10-30 meshes, drying the granular bergamot fruits until the moisture content is smaller than or equal to 13%, and using the obtained bergamot fruit powder as a raw material to extract the bergamot fruit essential oil through continuous phase transition at the low temperature, wherein the technology conditions include that the extraction temperature is 50-65 DEG C; the extraction pressure is 0.4-0.7MPa; the resolving temperature of a resolving pot is 55 DEG C and the pressure is 0.25MPa; the whole extraction time is 45-90 minutes; and the bulk density of the raw material of the bergamot fruit powder directly put in the extraction pot is 0.3-0.5 kg / L. The method disclosed by the invention summarizes technology conditions for extraction of the bergamot fruits through the continuous phase transition at the low temperature; in the whole extraction process, a high temperature does not exist so that active substances are not damaged, and hazardous substances such as polymers cannot be generated; the operation is convenient and safe; the method is environmental-friendly; and the method is quite suitable for continuous large-scale industrial production.

Description

technical field [0001] The invention relates to the technical field of extraction and separation, in particular to a method for extracting bergamot essential oil through continuous phase change at low temperature. Background technique [0002] The volatile essential oil content in bergamot is 16.0mL / kg, and its taste is delicate and elegant. It is an important high-grade spice plant and has been widely used in food and cosmetics abroad. The existing research results show that the main components of bergamot volatile essential oil are terpenes, sesquiterpenes, higher alcohols, aldehydes, ketones, esters and other physiologically active substances, which have high medicinal value. It has the effects of expectorant, cough, asthma, anti-anxiety, antibacterial and anti-inflammatory, and free radical removal. Bergamot essential oil contains various components such as limonene, γ-terpinene, α- and β-pinene, linalool, linalyl acetate, etc. These components make bergamot have variou...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
Inventor 周爱梅杨慧林敏浩刘欣
Owner SOUTH CHINA AGRI UNIV
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