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Manufacturing technique of industrial binder asphalt

A technology of binder asphalt and production process, which is applied in the direction of chemical processing of tar asphalt/petroleum asphalt/natural asphalt, etc., which can solve the problems of long process, high requirements for equipment valves, and high safety risks, and achieve the increase of adjustment flexibility , high product quality, and the effect of improving safety

Active Publication Date: 2015-08-12
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the domestic production of modified asphalt mainly adopts the traditional kettle-type heating high-temperature polymerization process. This process not only consumes a lot of energy, but also has a long process, and the bottom of the kettle is easy to coke. The production cycle is short, usually only more than 20 days per cycle.
This process requires a high temperature in the kettle, which often needs to be heated to above 400°C. This not only requires high requirements for equipment, pipelines, and valves, but also produces flash oil that is prone to spontaneous combustion and explosion, causing the flash oil tank and the middle tank to become the biggest safety risk. area
Therefore, the quality of asphalt products produced by this process is often not up to the requirements

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0023] A new type of production process for industrial binder asphalt, such as figure 1 As shown, the temperature of the asphalt sent from the asphalt tower is about 340°C, adjust the asphalt liquid level of the reactor, and the liquid level is generally controlled at 2 / 3 of the volume of the reactor (the volume of the reactor is 20m 3 ), and by controlling the inflow rate of asphalt, the reaction time is controlled to be 4 hours, and the temperature in the reactor is adjusted to 310°C by heating the reactor with a natural gas heating furnace. Reaction, at the same time, the mixed gas of nitrogen and oxygen (oxygen volume content is 0.05%) is heated to 300°C by a steam heater, and the flow rate is controlled at 27m 3 / h enters the reactor from the bottom of the reactor through the mixed gas distribution injector. The mixed gas injector is an annular tubular structure with a pipe diameter of 25mm and a size of 60% of the inner diameter of the reactor. The gas inlet port is fe...

Embodiment 2

[0026] The asphalt sent from the asphalt tower has a temperature of about 340°C. Adjust the asphalt liquid level of the reactor. The liquid level is generally controlled at 2 / 3 of the volume of the reactor (the volume of the reactor is 20m 3 ), and by controlling the inflow rate of asphalt, the reaction time is controlled to be 4 hours, and the temperature in the reactor is adjusted to 320 ° C by heating the reactor with a natural gas heating furnace. Reaction, at the same time, the mixed gas of nitrogen and oxygen (oxygen volume content is 4%) is heated to 300°C by a steam heater, and the flow rate is controlled at 27m 3 / h enters the reactor from the bottom of the reactor through the mixed gas distribution injector. The mixed gas injector is an annular tubular structure with a pipe diameter of 25mm and a size of 60% of the inner diameter of the reactor. The gas inlet port is fed from the bottom of the injector. A plurality of air outlets are evenly distributed on the annul...

Embodiment 3

[0029] The asphalt sent from the asphalt tower has a temperature of about 340°C. Adjust the asphalt liquid level of the reactor. The liquid level is generally controlled at 2 / 3 of the volume of the reactor (the volume of the reactor is 20m 3 ), control the reaction time to be 5 hours, adjust the temperature in the reactor to be 360°C by heating the reactor with a natural gas heating furnace, at the same time, start the stirrer, adjust the rotating speed at 150 rpm, and carry out the high-temperature polycondensation reaction. At the same time, nitrogen and After the mixed gas of oxygen (oxygen volume content is 5%) is heated to 350°C by a steam heater, the flow rate is controlled at 40m 3 / h enters the reactor from the bottom of the reactor through the mixed gas distribution injector. The mixed gas injector is an annular tubular structure with a pipe diameter of 25mm and a size of 60% of the inner diameter of the reactor. The gas inlet port is fed from the bottom of the injec...

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Abstract

The invention relates to a manufacturing technique of novel industrial binder asphalt, which comprises the following steps that asphalt is fed into a reaction kettle; a stirrer is started; with the temperature in the reaction kettle controlled at 300-360 DEG C, high temperature polycondensation is performed to synthesize the industrial binder asphalt; at the same time, a mixed gas of nitrogen and oxygen is injected to the reaction kettle from the bottom of the reaction kettle; free radicals in the asphalt are oxidized by oxygen in the mixed gas in a reaction process to improve the molecular weight of the asphalt; and light ingredients in the asphalt are brought out by the left mixed gas, and are called flash oil. According to the technique, the mixed gas of nitrogen and oxygen is introduced to the reaction kettle, and the reaction temperature can be reduced to around 300 DEG C from the traditional over 400 DEG C, so that energy is saved, the cost is lowered greatly, and a synthetic product is high in quality. In addition, the mixed gas is introduced to participate in the reaction, so that a situation that no flash burn or explosion of the flash oil occurs is ensured, and the safety of technological operation is improved accordingly.

Description

technical field [0001] The invention belongs to the tar processing industry, and specifically relates to a production process of industrial binder asphalt (the softening point is adjustable at 100-150°C). Background technique [0002] At present, domestic tar processing is gradually tending to scale. There are more than 10 domestic manufacturers with a processing scale of more than 500,000 tons per year, and asphalt products account for more than half of the output of tar processing products. So far, domestic coal tar pitch products Mainly asphalt products with a softening point of 110°C. [0003] At present, the domestic production of modified asphalt mainly adopts the traditional kettle-type heating high-temperature polymerization process. This process not only consumes a lot of energy, but also has a long process, and the bottom of the kettle is easy to coke. The production cycle is short, usually only more than 20 days per cycle. This process requires a high temperature...

Claims

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Application Information

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IPC IPC(8): C10C3/04
CPCC10C3/04
Inventor 李轩科徐兵董志军袁观明李保六崔正威张江
Owner WUHAN UNIV OF SCI & TECH
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