All-in-one ceramic heating member and preparation technology thereof
A technology of ceramic heating body and preparation process, which is applied in the field of preparation technology of ceramic heating body, and can solve the problems of restricting large-scale production, unstable product performance, and low production efficiency
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Embodiment 1
[0076] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0077] a. Mixing: first mix 70% Si by mass 3 N 4 , 9% MgO, 5% Y 2 o 3 , 5% Al 2 o 3 , 5% SiO 2 , 3% La 2 o 3 , 3% BN mixed and stirred evenly to make ceramic raw materials, and then 50% ceramic raw materials and 50% heating raw materials MoSi 2 Mix and stir evenly to make powder;
[0078] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 8 hours;
[0079] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0080] d. Hot die-casting molding: adding paraffin wax to the dried powder in step c, heating and stirring, stirring evenly to form a slurry, adding the slurry to a hot press for die-casting, and molding the powder to obtain a green ...
Embodiment 2
[0086] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0087] a, mixing: first mix Si with a mass percentage of 96% 3 N 4 , 1% MgO, 1% Y 2 o 3 , 0.5% Al 2 o 3 , 0.5% SiO 2 , 0.5% La 2 o 3 , 0.5% BN mixed and stirred evenly to make ceramic raw materials, and then 95% ceramic raw materials and 5% heating raw material TiC were mixed and stirred evenly to make powder;
[0088] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 11 hours;
[0089] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0090] d. Dry press forming: add the powder after drying in step c to a binder and mix and stir, mix evenly to form a powder, put the powder into a hydraulic press for dry press forming, and form the po...
Embodiment 3
[0096] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0097] a. Mixing: first mix Si with 80% mass percentage 3 N 4 , 6% MgO, 4% Y 2 o 3 , 4% Al 2 o 3 , 4% SiO 2 , 1% La 2 o 3 , 1% BN mixed and stirred evenly to make ceramic raw materials, and then 60% ceramic raw materials, 20% heating raw materials TiC, 20% heating raw materials MoSi 2 Mix and stir evenly to make powder;
[0098] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 14 hours;
[0099] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0100] d. Extrusion molding: add the powder after drying in step c to a binder and mix and stir, mix evenly to form a powder, put the powder into an extruder for extrusion molding, and mold t...
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