Medical low-temperature reversible temperature-indicating coating and preparation method thereof
A temperature-indicating coating and low-temperature technology, which is applied in the field of medical materials, can solve the problems of poor water resistance and dry-erase performance, and achieve the effects of good heat resistance, good brushability, and simple and easy-to-obtain raw materials
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Embodiment 1
[0022] Step 1: Weigh 100 parts of epoxy-modified silicone resin, 5 parts of lead dioxide, 1 part of ethyl cellulose, 10 parts of cadmium carbonate, 15 parts of calcium fluoride, and 4 parts of talcum powder according to the ratio of parts by mass , 12 parts of barium sulfate, 1 part of Sudan orange, 0.5 part of titanium dioxide, and 1 part of red cyanine.
[0023] Step 2: Put epoxy-modified silicone resin, lead dioxide, ethyl cellulose, cadmium carbonate and talcum powder into the reaction kettle, and stir for 30 minutes at a speed of 400 r / min.
[0024] Step 3: Put the stirred liquid aside for 26 hours, add calcium fluoride, barium sulfate, Sudan orange, titanium dioxide and red cyanine, mix well, put it into a grinder and grind for 40 minutes.
[0025] The product is a reversible single color change at 70-90°C, the color changes from red to purple, and from purple to orange at 140-180°C; the product has a viscosity of 60s, water resistance 3d, no foaming, non-toxic, good hea...
Embodiment 2
[0027] Step 1: Weigh 100 parts of epoxy-modified silicone resin, 25 parts of lead dioxide, 20 parts of ethyl cellulose, 30 parts of cadmium carbonate, 35 parts of calcium fluoride, and 16 parts of talcum powder according to the ratio of parts by mass , 18 parts of barium sulfate, 5 parts of Sudan orange, 2.5 parts of titanium dioxide, and 3 parts of red cyanine.
[0028] Step 2: put epoxy-modified silicone resin, lead dioxide, ethyl cellulose, cadmium carbonate and talcum powder into the reaction kettle, and stir for 50 minutes at a speed of 600 r / min.
[0029] Step 3: Leave the stirred liquid to stand for 30 hours, add calcium fluoride, barium sulfate, Sudan orange, titanium dioxide and red cyanine, mix well, put it into a grinder and grind for 60 minutes.
[0030] The product is a reversible single color change at 70-90°C, the color changes from red to purple, and from purple to orange at 140-180°C; the product has a viscosity of 65s, a water resistance of 4d, no foaming, no...
Embodiment 3
[0032] Step 1: Weigh 100 parts of epoxy-modified silicone resin, 10 parts of lead dioxide, 5 parts of ethyl cellulose, 15 parts of cadmium carbonate, 20 parts of calcium fluoride, and 6 parts of talcum powder according to the ratio of parts by mass , 14 parts of barium sulfate, 2 parts of Sudan orange, 1 part of titanium dioxide, and 1.5 parts of red cyanine.
[0033] Step 2: Put epoxy-modified silicone resin, lead dioxide, ethyl cellulose, cadmium carbonate and talcum powder into the reaction kettle, and stir for 35 minutes at a speed of 450 r / min.
[0034] Step 3: Put the stirred liquid aside for 27 hours, add calcium fluoride, barium sulfate, Sudan orange, titanium dioxide and red cyanine, mix well, put it into a grinder and grind for 45 minutes.
[0035] The product is a reversible single color change at 70-90°C, the color changes from red to purple, and from purple to orange at 140-180°C; the product has a viscosity of 70s, water resistance of 5d, no foaming, non-toxic, g...
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