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A kind of preparation method of annular elastic ring of medical ligation device

A technology for elastic rings and ligation devices, which is applied in the field of preparation of annular elastic rings for medical ligation devices, can solve problems such as easy inflammation and pain, poor compatibility with human tissue, and general anti-wet skid performance, and achieve good pro- Effect of water properties and anti-wet skid properties, good medical prospects, excellent mechanical properties

Active Publication Date: 2017-06-06
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, when natural rubber is used for the rubber ring of the ligation device, there are still some shortcomings such as poor compatibility with human tissue, easy inflammation and pain, general anti-wet skid performance, high permanent deformation, and easy to fall off, making natural rubber Applications in this area are limited
At present, there are few reports on the use of natural rubber in the aprons of medical ligation devices

Method used

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  • A kind of preparation method of annular elastic ring of medical ligation device
  • A kind of preparation method of annular elastic ring of medical ligation device
  • A kind of preparation method of annular elastic ring of medical ligation device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] The preparation method of the medical ligation device annular elastic ring of the present embodiment is as follows:

[0038] (1) Weigh 100 parts of Malaysian tobacco sheet glue, 2.0 parts of medical stearic acid, 5.0 parts of medical zinc oxide, 2.0 parts of accelerator TMTD, 2.0 parts of anti-aging agent 264, 0.5 parts of medical paraffin, 3.0 parts of glycerin, medical 10.0 parts of gas-phase hydrophilic white carbon black, 0.8% of titanate coupling agent 105, 1.0 parts of medical PPO, and 2.0 parts of sulfur.

[0039] (2) Carry out plasticizing completely to the Malaysian smoked sheet rubber;

[0040] (3) Add medical stearic acid, medical zinc oxide and medical paraffin to the product obtained in step (2), and knead evenly;

[0041] (4) Add medical PPO and glycerin to the product of step (3), and mix evenly;

[0042] (5) Add titanate coupling agent 105 to the product obtained in step (4), and knead evenly;

[0043] (6) Add medical gas-phase hydrophilic white carbo...

Embodiment 2

[0053] The preparation method of the medical ligation device annular elastic ring of the present embodiment is as follows:

[0054] (1) Weigh 100 parts of quasi-rubber No. 5 rubber, 3.0 parts of medical stearic acid, 6.0 parts of medical zinc oxide, 1.0 parts of accelerator TMTM, 3.0 parts of anti-aging agent RD, 0.5 parts of medical paraffin, and 5.0 parts of glycerin , 30 parts of medical vapor phase hydrophobic white carbon black, coupling agent Si69 1.5%, 2.0 parts of medical PEG, 1.5 parts of sulfur.

[0055] (2) Carry out mastication completely to standard rubber No. 5 natural rubber raw rubber;

[0056] (3) Add medical stearic acid, medical zinc oxide and medical paraffin to the product obtained in step (2), and knead evenly;

[0057] (4) Add medical PEG and glycerol to the product obtained in step (3), and mix evenly;

[0058] (5) Add coupling agent Si 69 to the product obtained in step (4), and mix evenly;

[0059] (6) Add medical vapor-phase hydrophobic white carb...

Embodiment 3

[0069] The preparation method of the annular elastic ring of the medical ligation device of this embodiment is the same as that of Embodiment 1 except for the formula.

[0070] The formula of the medical ligation device annular elastic ring of the present embodiment is as follows: 100 parts of first-grade thin white crepe film, 2.0 parts of medical stearic acid, 5.0 parts of medical zinc oxide, 1.5 parts of accelerator TETD, 4.0 parts of anti-aging agent MB, medical 0.5 parts of paraffin, 3.0 parts of glycerin, 15 parts of medical precipitated white carbon black, 3.0 parts of medical PVA, and 2.0 parts of sulfur.

[0071] The test results of the annular elastic ring of the medical ligation device prepared in this embodiment are shown in Table 3.

[0072] table 3

[0073] Test items unit value Tensile Strength MPa 30 elongation at break % 840 hardness Shore A 55 permanent deformation % 8 Contact angle ° 53

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Abstract

The invention discloses a preparation method of an annular elastic ring of a medical ligator. The method comprises the following steps: with natural rubber as a raw material, adding a certain ratio of active agent, and mixing completely; adding a hydrophilic material, a coupling agent and white carbon black, and mixing evenly; and finally adding a medical accelerant, an anti-aging agent and a vulcanizing agent and carrying out vulcanization and hot press molding. The annular elastic ring of the medical ligator disclosed by the invention is good in biocompatibility, has certain hydrophilic properties, and is small in permanent deformation and firm in ligation; and the tissue is stable to fall off. The annular elastic ring of the medical ligator disclosed by the invention can be applied to the ligation operation of haemorrhoids in the field of bio-medical treatment; materials are convenient to draw; the operation is simple; and the preparation method is poisonless and harmless, and has a good medical prospect.

Description

technical field [0001] The invention relates to the field of preparation of rubber rings, in particular to a preparation method of an annular elastic ring of a medical ligation device. Background technique [0002] Because of its good elasticity and mechanical strength, natural rubber is widely used in the electronics industry, construction industry, automobile industry, medical treatment and aerospace industries. In the medical industry, it is often used as catheters, rubber plugs and ligation rubber rings. [0003] Hemorrhoids are a very common clinically common anorectal disease. Although they are not fatal, they can occur at any time and affect people's lives and health. 90% of rectal cancers are misdiagnosed as hemorrhoids at the early stage, and visible hemorrhoids cannot be ignored. With the development of medical technology, the treatment of hemorrhoids is becoming more and more mature. The most effective treatment methods currently recognized mainly include: one i...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L7/00C08K13/02C08K5/09C08K3/22C08K3/36C08K5/053
CPCB29C35/02C08L7/00C08L2203/02C08L2205/025C08L2205/03C08L91/06C08L71/02C08K13/02C08K5/09C08K2003/2296C08K3/36C08K5/053C08K3/06C08L29/04C08L89/00C08K5/5435
Inventor 刘卅任力靳德道王迎军王磊王辉
Owner SOUTH CHINA UNIV OF TECH