A kind of nanofiber multi-layer composite filter mask and preparation method thereof
A nanofiber and multi-layer composite material technology, applied in the field of daily necessities, can solve problems such as unsatisfactory, large specific surface area, and large influence range, and achieve the effect of improving filtration efficiency and good air permeability
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Embodiment 1
[0030] The present invention, a kind of preparation method of nanofiber multilayer composite filter mask, it specifically comprises the following steps:
[0031] Step 1, dissolving the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer nanofiber solution with a mass fraction of 15%;
[0032] Step 2. Add the polymer nanofiber solution in step 1 into the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290mm, and PP spunbonded non-woven fabric is selected as the receiving substrate, and the operating speed of the substrate is 450mm / min, obtain the monomer material of spunbonded nonwoven fabric and polymer nanofiber, wherein the diameter of polymer nanofiber is about 60nm;
[0033] Step 3. Compound the above monomer materials in three layers to obtain a three-layer composite material. After testing, the filtration efficiency of this three-layer composite material can reach 90%, and the resistance is about 9mmH 2 O, meet ...
Embodiment 2
[0035] The present invention, a kind of preparation method of nanofiber multilayer composite filter mask, it specifically comprises the following steps:
[0036] Step 1, dissolving the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer solution with a mass fraction of 15%;
[0037] Step 2, add the polymer nanofiber solution in step 1 to the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290mm, and the melt-blown non-woven fabric is selected as the receiving substrate, and the operating speed of the substrate is 400mm / min, one side of the melt-blown non-woven fabric is coated to obtain a monomer material of the melt-blown non-woven fabric and polymer nanofibers;
[0038] Step 3. Coating the other side of the monomer material on one side of the above-mentioned coating with polymer nanofibers, the method is the same as step 2, and after coating, a composite material coated with polymer nanofibers on both sides is obtain...
Embodiment 3
[0040] The present invention, a kind of preparation method of nanofiber multilayer composite filter mask, it specifically comprises the following steps:
[0041] Step 1. Dissolve the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer solution with a mass fraction of 15%, called polymer nanofiber solution 1; dissolve the weighed PVDF in N, N -In dimethylformamide (DMF) solvent, be prepared into the polymer solution that mass fraction is 18%, be called polymer nanofiber solution two;
[0042] Step 2. First, add the polymer nanofiber solution to the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290mm, the PP non-woven fabric is the receiving substrate, and the operating speed of the substrate is 450mm / min, and the obtained Monomer material 1 of nylon 6 and PP non-woven fabric, in which the diameter of nylon 6 nanofiber is about 60nm;
[0043]Step 3. Add the polymer nanofiber solution 2 to the electrospinning device, th...
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Abstract
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