Aluminum tellurium master alloy and its preparation method and application
A technology of aluminum-tellurium master alloy and master alloy, which is applied in the field of aluminum-tellurium master alloy and its preparation, can solve the problems of tellurium segregation and precipitation, difficulty in control, deposition at the bottom of the crucible, etc., achieve stable and accurate yield, and not easy to burn and oxidize , Reduce the effect of burning loss and oxidation
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Embodiment 1
[0034] The preparation method of the aluminum-tellurium master alloy described in this embodiment is as follows:
[0035] (1) Ingredients
[0036] Using tellurium and aluminum as raw materials, the mass fraction of tellurium in the aluminum-tellurium master alloy is 0.1%, and the mass fraction of aluminum is 99.9% to weigh the raw materials;
[0037] (2) Melting
[0038] After preheating aluminum in a heating furnace to remove adsorbed moisture and gas, add a covering agent of 0.5% of the total mass of aluminum and tellurium, the covering agent is obtained by mixing sodium chloride and potassium chloride at a mass ratio of 1:1 The mixture is heated to melt all the aluminum to obtain aluminum liquid, and then the tellurium is pressed into the aluminum liquid in batches with a bell jar at 680 ° C. The amount added each time is 3% of the total amount of tellurium. After all the tellurium is added and melted, Keep stirring at 680°C for 5 minutes, then remove slag, keep the tempe...
Embodiment 2
[0042] The preparation method of the aluminum-tellurium master alloy described in this embodiment is as follows:
[0043] (1) Ingredients
[0044] Using tellurium and aluminum as raw materials, the mass fraction of tellurium in the aluminum-tellurium master alloy is 1.0%, and the mass fraction of aluminum is 99.0% to weigh the raw materials;
[0045] (2) Melting
[0046]After the aluminum is preheated in a heating furnace to remove the adsorbed moisture and gas, 1.0% of the total mass of aluminum and tellurium is added as a covering agent potassium chloride, heated to melt all aluminum to obtain aluminum liquid, and then batched at 720 ° C. Press the tellurium into the molten aluminum with a bell jar, and the amount of each addition is 5% of the total amount of tellurium. After all the tellurium is added and melted, keep stirring at 700 ° C for 10 minutes, and then remove the slag. Adding 0.7% of the total mass of aluminum and tellurium to the aluminum and tellurium melts af...
Embodiment 3
[0050] The preparation method of the aluminum-tellurium master alloy described in the present embodiment is as follows:
[0051] (1) Ingredients
[0052] Using tellurium and aluminum as raw materials, the raw materials are weighed according to the mass fraction of tellurium in the aluminum-tellurium master alloy is 10.0% and the mass fraction of aluminum is 90.0%;
[0053] (2) Smelting
[0054] After the aluminum is preheated in a heating furnace to remove the adsorbed moisture and gas, 1.0% of the total mass of aluminum and tellurium is added as a covering agent potassium chloride, heated to melt all aluminum to obtain aluminum liquid, and then batched at 720 ° C. Press the tellurium into the molten aluminum with a bell jar, and the amount of each addition is 5% of the total amount of tellurium. After all the tellurium is added and melted, keep stirring at 700 ° C for 10 minutes, and then remove the slag. Adding 0.7% of the total mass of aluminum and tellurium to the alumin...
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