A corrosion method for ultra-high pressure energy storage materials
An energy storage material and ultra-high voltage technology, applied in the direction of electrolytic capacitors, capacitors, electrical components, etc., can solve the problems of easy clogging specific volume, small holes in corroded foil, etc., to overcome small holes, fast boost time, and good mechanical strength and the effect of service life
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Embodiment 1
[0040] 1. Preparation of raw material aluminum foil: select the aluminum foil prepared by vacuum annealing at 550°C for 1 hour as the raw material, with a cubic texture ≥ 96% and a thickness of 116 μm; the chemical composition of the raw material aluminum foil is shown in Table 1.
[0041] The chemical composition of table 1 raw material aluminum foil (mass fraction, %)
[0042]
[0043] Two, adopt the method of the present invention to prepare corroded foil, comprise the following steps:
[0044] (1) Pretreatment: first soak the raw material aluminum foil in 0.8mol / L sodium hydroxide solution for 60s, control the treatment temperature at 50°C; then soak the aluminum foil in a mixed solution containing 3wt% sulfuric acid and 5wt% phosphoric acid for 120s , control the treatment temperature at 60°C; finally use deionized water to wash the aluminum foil at room temperature for 2 minutes;
[0045] (2) One-level direct-current electrochemical corrosion: place the aluminum foil...
Embodiment 2
[0053] 1. Preparation of raw material aluminum foil: select the aluminum foil prepared by vacuum annealing at 530°C for 1.5h as the raw material, with a cubic texture ≥ 95% and a thickness of 110 μm; the chemical composition of the raw material aluminum foil is shown in Table 2.
[0054] The chemical composition of table 2 raw material aluminum foil (mass fraction, %)
[0055]
[0056] Two, adopt the method of the present invention to prepare corroded foil, comprise the following steps:
[0057] (1) Pretreatment: first soak the raw material aluminum foil in 1mol / L sodium hydroxide solution for 50s, control the treatment temperature to 455°C; then soak the aluminum foil in a mixed solution containing 5wt% sulfuric acid and 3wt% phosphoric acid for 150s, Control the treatment temperature at 50°C; finally use deionized water to wash the aluminum foil at room temperature for 3 minutes;
[0058] (2) First-level direct current electrochemical corrosion: place the aluminum foil t...
Embodiment 3
[0066] 1. Preparation of raw material aluminum foil: select the aluminum foil prepared by vacuum annealing at 580°C for 0.5h as the raw material, with a cubic texture ≥ 95% and a thickness of 120 μm; the chemical composition of the raw material aluminum foil is shown in Table 3.
[0067] The chemical composition of table 3 raw material aluminum foil (mass fraction, %)
[0068]
[0069] Two, adopt the method of the present invention to prepare corroded foil, comprise the following steps:
[0070] (1) Pretreatment: first soak the raw material aluminum foil in 0.5mol / L sodium hydroxide solution for 80s, control the treatment temperature at 60°C; then soak the aluminum foil in a mixed solution containing 2wt% sulfuric acid and 8wt% phosphoric acid for 60s , control the treatment temperature to 70°C; finally use deionized water to wash the aluminum foil at room temperature for 2 minutes;
[0071] (2) One-level direct-current electrochemical corrosion: place the aluminum foil tr...
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