LED epitaxial layer growing method and LED epitaxial wafer and LED chip obtained by same
An LED epitaxial wafer and LED chip technology, applied in electrical components, circuits, semiconductor devices, etc., can solve problems such as luminous efficiency attenuation, and achieve the effects of improving luminous efficiency attenuation, reducing blocking effect, and improving brightness
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[0041] The specific preparation method is described as follows: Aixtron Cruis I MOCVD (metal organic chemical vapor deposition method) is used to grow the LED epitaxial wafer with the above structure. Using high-purity H 2 and / or N 2 As a carrier gas, high-purity NH 3 As the N source, the metal-organic source trimethylgallium (TMGa), triethylgallium is used as the gallium (TEGa) source, trimethylindium (TMIn) is used as the indium source, and the N-type dopant is silane (SiH 4 ), the P-type dopant is magnesocene (CP2Mg), the substrate is (0001) plane sapphire, and the reaction pressure is 100mbar-800mbar.
[0042] 1. Raise the temperature to 1100°C, and maintain the pressure of the reaction chamber at 150mbar to treat the sapphire substrate at high temperature for 5 minutes in a hydrogen atmosphere;
[0043] 2. Cool down to 550°C, maintain the pressure of the reaction chamber at 600mbar, and grow a low-temperature buffer layer GaN with a thickness of 30nm on the sapphire su...
Embodiment 1
[0054] 1. Raise the temperature to 1100°C, and maintain the pressure of the reaction chamber at 150mbar to treat the sapphire substrate at high temperature for 5 minutes in a hydrogen atmosphere;
[0055] 2. Cool down to 550°C, maintain the pressure of the reaction chamber at 600mbar, and grow a low-temperature buffer layer GaN with a thickness of 30nm on the sapphire substrate;
[0056] 3. Raise the temperature to 1050°C, maintain the pressure in the reaction chamber at 600mbar, and continue to grow 3μm undoped GaN;
[0057] 4. Then continue to grow N-type GaN doped with Si, the Si doping concentration is 1E+19atom / cm3, and the total thickness is controlled at 4μm;
[0058] 5. Periodically grow the active layer MQW, maintain the pressure of the reaction chamber at 300mbar, (1) cool down to 750°C, and grow In with a thickness of 3.2nm 0.25 Ga 0.75 N well layer; (2) increase the temperature to 850°C, and grow a GaN barrier layer with a thickness of 12nm; repeat the growth ste...
Embodiment 2
[0064] The difference with embodiment 1 is:
[0065] 6. Periodically grow a superlattice layer as an electron blocking layer, control the temperature at 1000°C, control the pressure in the reaction chamber at 600mbar, and grow 2nm P-type In 0.2 Ga 0.8 N layer and 2nm P-type Al 0.02 Ga 0.98 N layer, Mg doping concentration 1E+20; change the TMIn and TMAl doping concentration of the MOCVD (metal organic chemical vapor deposition) reaction chamber, and continue to grow 2nm P-type In 0.18 Ga 0.82 N layer and 2nm P-type Al 0.04 Ga 0.96 N layer, Mg doping concentration is 1E+20; (other steps not described in detail are the same as in Example 1); according to the above method, 10 cycles of In x Ga (1-x) N / Al y Ga (1-y) N superlattice electron blocking layer, where x is 0.2, 0.18, 0.16, 0.14, 0.12, 0.1, 0.08, 0.06, 0.04, 0.02, y is 0.02, 0.04, 0.06, 0.08, 0.1, 0.12, 0.14, 0.16 , 0.18, 0.2, the total thickness of the electron blocking layer is 40nm.
[0066] Other steps rema...
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