A kind of fiber and its preparation method and prepared fabric
A fiber and primary fiber technology, applied in the field of fabric fibers, can solve the problems of long yellowing resistance, high temperature resistance, ultraviolet resistance, yellowing resistance, etc., and achieves stable quality performance, reliable safety, and good uniformity. Effect
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Embodiment 1
[0048] A fiber prepared by the following method:
[0049] Get the following raw materials by weight percentage for subsequent use, polycondensate of m-phenylene isophthalamide 94%, polyamide 3%, anti-yellowing agent 1.5%, anti-ultraviolet agent 1.5%;
[0050] After the raw materials are mixed, calcium hydroxide is added to carry out neutralization reaction to obtain a polymer containing 17% and 5% CaCl 2 viscous liquid;
[0051] The viscous liquid is filtered and heated to 165°C for dry spinning to obtain primary fibers;
[0052] The as-spun fibers are washed with water to remove inorganic salts, and then stretched 4 times at 290°C.
[0053] The breaking strength of the prepared fiber is 0.4-0.5 N / tex, the elongation is 30-50%, and the moisture regain is 5-6.5%. According to ISO 105 / B02 of the International Organization for Standardization, the yellowing resistance of the fiber reaches GRADE6; The anti-ultraviolet radiation reaches the A level in the international AS / NZS439...
Embodiment 2
[0056] A fiber prepared by the following method:
[0057] Get the following raw materials by weight percentage for subsequent use, polycondensate of m-phenylene isophthalamide 90%, polyamide 5%, anti-yellowing agent 3%, anti-ultraviolet agent 2.0%;
[0058] The polycondensate of m-phenylene isophthalamide is prepared by low-temperature solution polycondensation method, dissolving m-phenylene diamine in N, N dimethylacetamide solvent, adding isophthaloyl chloride under stirring, and reacting to obtain spinning silk liquid;
[0059] Add polyamide, anti-yellowing agent and anti-ultraviolet agent to the spinning solution, add calcium hydroxide to carry out neutralization reaction after mixing, obtain the polymer containing 18% and 6% CaCl 2 viscous liquid;
[0060] The viscous liquid is filtered and heated to 170°C for dry spinning to obtain primary fibers;
[0061] The as-spun fibers are washed with water to remove inorganic salts, and then stretched 4 times at 285°C.
[0062...
Embodiment 3
[0065] A fiber prepared by the following method:
[0066] Get the following raw materials by weight percentage for subsequent use, polycondensate of m-phenylene isophthalamide 92%, polyamide 4%, anti-yellowing agent 2%, anti-ultraviolet agent 2.0%;
[0067] After the raw materials are mixed, calcium hydroxide is added to carry out neutralization reaction to obtain a polymer containing 18% and 6% CaCl 2 viscous liquid;
[0068] The viscous liquid is filtered and heated to 175°C for dry spinning to obtain primary fibers;
[0069] The as-spun fibers are washed with water to remove inorganic salts, and then stretched 5 times at 290°C.
[0070] The breaking strength of the prepared fiber is 0.4-0.5 N / tex, the elongation is 30-50%, and the moisture regain is 5-6.5%. According to ISO 105 / B02 of the International Organization for Standardization, the yellowing resistance of the fiber reaches GRADE6; The anti-ultraviolet radiation reaches the A level in the international AS / NZS4399 ...
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