Identification method for aromatic cacao breeding material
An identification method and aroma type technology, applied in the field of biological information, can solve the problems of wrong identification, lack of universality, lack of accurate identification technology of cocoa aroma quality, etc., and achieve the effects of strong practicability, high accuracy and short analysis time.
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Embodiment 1
[0054] Example 1: Common cocoa CCN51 verifies the identification method of the present invention
[0055] Considering that the degree of fermentation and roasting of cocoa beans has a large difference in their aroma, and cannot reflect the precursor substances of cocoa aroma, in order to avoid the influence of these factors on the aroma of cocoa, the present invention requires that the cocoa sample is not fermented and roasted. .
[0056] Accurately weigh 500g-1000g cocoa beans that have not been fermented, roasted and have a moisture content of less than 8%, put them in a stainless steel mortar, pulverize, pass through a 40-mesh sieve, and stand by.
[0057] Detection of aroma components in cocoa samples:
[0058] A). Extraction head selection and aging: choose 50 / 30μm, divinylbenzene / carbon molecular sieve / polydimethylsiloxane (DVB / CAR / PDMS) solid phase microextraction (SPME) fiber head; SPME before use The extraction head is aged at the inlet of the gas chromatography (GC), the ag...
Embodiment 2
[0088] Example 2: Ecuadorian flavored cocoa arribaNacional verifies the identification method of the present invention
[0089] The selection of known cocoa beans is shown in Table 3. The detection of aroma components in other cocoa samples, the identification of aroma substances in cocoa samples and the establishment of data matrix, the ANOSIM difference test between aromatic cocoa and common cocoa, the difference between aromatic cocoa and common cocoa The clustering analysis and other steps are the same as in Example 1;
[0090] ANOSIM analysis results show that the aroma composition of fragrant cocoa and ordinary cocoa is significantly different (R=0.3991, n=12, p=0.015).
[0091] Cocoa testing to be tested:
[0092] GC / MS was used to detect the aroma composition and content of the Ecuadorian cocoa arribaNacional variety, and all the GC / MS aroma substance confidence of arriba cocoa samples were converted to export data, and compiled into the "m×(K+12) formed in Example 1. )” matr...
Embodiment 3
[0097] Example 3: Dominican flavored cocoa Hispaniola Trinitario variety verification The identification method of the present invention
[0098] See Table 4 for the selection of known cocoa beans, detection of aroma components in cocoa samples, identification of aroma substances in cocoa samples and establishment of data matrix, ANOSIM difference test between aromatic cocoa and common cocoa, and aromatic cocoa and common cocoa Class analysis is the same as in Example 1;
[0099] Identification of aroma substances in cocoa samples and establishment of data matrix:
[0100] Same as Example 1, the "m×(K+9)" matrix is shown in Table 4.
[0101] Table 4 Identification and content of aroma components of fragrant cocoa samples (FC) and common cocoa samples (BC) based on GC / MS technology (μg·kg -1 FW) analysis
[0102]
[0103]
[0104] The results of ANOSIM analysis showed that the aroma composition of fragrant cocoa and ordinary cocoa was significantly different (R=0.4875, n=9, p=0.023). ...
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