Preparing method of antibacterial acrylic fiber color silk

A technology of colored silk and acrylic fiber, which is applied in the field of special synthetic fiber preparation, can solve the problems of increasing environmental pollution, large printing and dyeing sewage, and high energy consumption, and achieves the effects of good physical properties, wide application and high color fastness.

Inactive Publication Date: 2015-12-09
SHANGHAI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method uses alkali to treat fibers, consumes a lot of energy and increases environmental pollution, and the use of antibacterial agents containing halogen elements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] In the present embodiment, a kind of preparation method of antibacterial acrylic colored yarn, the steps are as follows:

[0024] a. Polyacrylonitrile powder 100g is dissolved in concentration and is in the sodium thiocyanate solution of 51wt%, then 1g nano-titanium dioxide antibacterial agent is added in the solution, makes spinning dope;

[0025] b. Vibrate the spinning stock solution prepared in step a for 4 hours in an ultrasonic wave, and defoam;

[0026] c. The preparation multistage coagulation bath comprises a first-level coagulation bath, a second-level coagulation bath and a three-level coagulation bath, specifically: in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 11wt% sodium thiocyanate solution as a Level coagulation bath; in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 2wt% sodium thiocyanate solution as a secondary coagulation bath; in deionized...

Embodiment 2

[0038] This embodiment is basically the same as Embodiment 1, especially in that:

[0039] In the present embodiment, a kind of preparation method of antibacterial acrylic colored yarn, the steps are as follows:

[0040] a. Polyacrylonitrile powder 100g is dissolved in concentration and is in the solution of 51wt% sodium thiocyanate, then 1.5g nano titanium dioxide antibacterial agent is added in the solution, makes spinning dope;

[0041] b. This step is identical with the step of embodiment one;

[0042] c. The preparation multistage coagulation bath comprises a first-level coagulation bath, a second-level coagulation bath and a three-level coagulation bath, specifically: in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 10wt% sodium thiocyanate solution as a Level coagulation bath; in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 1.5wt% sodium thiocyanate solution as...

Embodiment 3

[0053] This embodiment is basically the same as the previous embodiment, and the special features are:

[0054] In the present embodiment, a kind of preparation method of antibacterial acrylic colored yarn, the steps are as follows:

[0055] a. Polyacrylonitrile powder 100g is dissolved in concentration and is in the sodium thiocyanate solution of 51wt%, then 1g nano-titanium dioxide and 1.5 gram nano-silver are added in the solution, make spinning dope;

[0056] b. This step is identical with the step of embodiment one;

[0057] c. The preparation multistage coagulation bath comprises a first-level coagulation bath, a second-level coagulation bath and a three-level coagulation bath, specifically: in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 10wt% sodium thiocyanate solution as a Level coagulation bath; in deionized water, adjust the pH value to 5 with glacial acetic acid, and prepare a concentration of 2wt% sodium t...

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PUM

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Abstract

The invention discloses a preparing method of an antibacterial acrylic fiber color silk. Spinning, coloring and antibiosis finishing are finished in one step. The method comprises the steps of firstly, blending an antibacterial agent in a wet spinning dope, molding in coagulating bath by extruding to obtain primary acrylic fiber, and then performing anion dye gel coloring to prepare the antibacterial agent-loaded acrylic fiber color silk. The antibacterial function finishing and fiber coloring are realized in one step to prepare the acrylic fiber color silk with the antibacterial function, the antibacterial agent is introduced into polyacrylonitrile fiber by adopting a dope spinning method, the antibacterial effect is good and durable, and a post finishing process is reduced; the acrylic fiber color silk obtained by a gel dyeing method is good in color brightness, high in color fastness and capable of reducing dyeing sewage.

Description

technical field [0001] The invention relates to a preparation method of colored textile fibers, in particular to a preparation method of colored functional textile fibers, which is applied in the technical field of preparation of special synthetic fibers. Background technique [0002] Acrylic fiber is a very important raw material in the textile industry. It has a large output and a wide range of uses. It is also called the three major synthetic fibers together with polyester and nylon. Acrylic fiber has the characteristics of wool. It has good bulkiness and warmth retention, soft hand feeling, excellent light resistance and other characteristics. It has been widely used in textiles such as textiles, clothing, car seats, and household curtains. However, with the improvement of people's living standards, when acrylic fiber is used in textile products, in addition to the comfort, beauty, economical and durable performance required by traditional textiles, it often puts forward...

Claims

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Application Information

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IPC IPC(8): D01F6/54D01F1/10D06P1/41D06P1/673D06P1/66D06P3/76D01D1/02D01D5/06D01D10/00D01D4/02
Inventor 俞成丙伍芳芳石小龙虞玺聂娅董海涛
Owner SHANGHAI UNIV
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