Application of phosphoric acid ester compound to flotation of calcium-containing minerals

A phosphate ester and mineral flotation technology, applied in flotation, solid separation, etc., can solve the problems of small dosage of chemicals, difficulty in flotation and separation of minerals containing calcium salts, etc., achieve low production cost, low cost, and meet the requirements of industrial The effect of production

Active Publication Date: 2015-12-16
CENT SOUTH UNIV
3 Cites 15 Cited by

AI-Extracted Technical Summary

Problems solved by technology

[0006] For the flotation process of calcium-containing salt minerals in the prior art, the surface chemical composition of calcium-containing minerals is similar to that of the flotation agent and the reactivity with the agent is similar, resulting in difficulties in the flotation separation of calcium-containing salt minerals. The purpose of the present invention is to provide a kind of phosphoric acid ester compound as the applic...
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Method used

Above-mentioned gained phosphoric acid ester compound is used as Chen Fluorite and calcite flotation separation, and table 1 is the comparison result of new medicament and traditional calcite inhibitor acidified water glass, and the result shows that new preparation has extremely strong selectivity to calcite inhibition.
Above-mentioned gained ...
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Abstract

The invention discloses an application of a phosphoric acid eater compound to flotation of calcium-containing minerals. The phosphoric acid eater compound replaces traditional water glass to serve as a calcite inhibitor for the flotation of the calcium-containing minerals. The phosphoric acid eater compound has a selective inhibiting effect on calcite, and is particularly suitable for flotation of fluorite, scheelite, apatite, cassiterite and other minerals. In addition, the phosphoric acid eater compound has the characteristics of being good in inhibiting effect, stable in property, small in usage amount and low in cost so that the quality of concentrate of the scheelite, the fluorite and the apatite can be effectively improved.

Application Domain

Flotation

Technology Topic

Selective inhibitionCalcite +8

Image

  • Application of phosphoric acid ester compound to flotation of calcium-containing minerals
  • Application of phosphoric acid ester compound to flotation of calcium-containing minerals
  • Application of phosphoric acid ester compound to flotation of calcium-containing minerals

Examples

  • Experimental program(2)

Example Embodiment

[0027] Example 1
[0028] In a 300mL three-necked flask equipped with a stirrer, thermometer, condenser, and dropping funnel, add 10g ethylene glycol, 40g ethylene glycol monoethyl ether, 40g polyoxyethylene ether glycerol (molecular weight 1500), 30g ethylene glycol mono Diethyl ether, heated to 75℃ under stirring and mixing, then slowly add 20g of phosphorus pentoxide, control the reaction temperature to reach 130-140℃ after adding phosphorus pentoxide, and then add 30g of ethylene glycol monoethyl ether, and add it to 140 Keep the temperature at ℃ for 1h, add water to cool the product, and get the required calcite inhibitor. Its infrared spectrum analysis such as figure 1. It is used to separate calcite from fluorite flotation.
[0029] The phosphate compound obtained above was used for the flotation separation of fluorite and calcite. Table 1 shows the comparison results of the new agent and the traditional calcite inhibitor acidified water glass. The results show that the new agent has a strong selective inhibitory effect on calcite.
[0030] Table 1 Comparison results of acidified water glass with new agent and traditional calcite inhibitor
[0031]
[0032] The aminophosphonic acid compound is used for the separation of scheelite and fluorite ore. The fluorite concentrate contains 95% fluorite and 1.26% tungsten. Sodium oleate (500g/t) is used as collector, aminophosphonic acid compound (100g/t) is used to inhibit scheelite to obtain 99% fluorite concentrate and 4.58% tungsten containing 89% fluorite Tungsten concentrate.

Example Embodiment

[0033] Example 2
[0034] In a 300mL three-necked flask equipped with a stirrer, thermometer, condenser, and dropping funnel, add 10g ethylene glycol, 40g ethylene glycol monoethyl ether, 40g polyoxyethylene ether glycerol (molecular weight 1200), 30g ethylene glycol mono Diethyl ether, heated to 80℃ under stirring and mixing, then slowly add 20g phosphorus pentoxide, control the reaction temperature to reach 130-140℃ after adding phosphorus pentoxide, then add 30g ethylene glycol monoethyl ether, and add it to 140 Keep the temperature at ℃ for 2h, add water to cool the product, and get the required calcite inhibitor. Its infrared spectrum analysis such as figure 1. It is used to separate calcite from fluorite flotation.
[0035] The phosphate compound obtained above was used for the flotation separation of Shizhuyuan tungsten ore and calcite. Table 2 shows the comparison results of the new agent and the traditional calcite inhibitor salted water glass. The results show that the new agent is used in the flotation process of tungsten ore with calcite. It has a strong selective inhibitory effect.
[0036] Table 2 Comparison results of new agent and traditional calcite inhibitor salted water glass
[0037]
[0038]
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Description & Claims & Application Information

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