Formula and preparing method of carbon fiber sizing agent for reinforcing polypropylene

A carbon fiber and polypropylene technology, which is applied to the formulation and preparation field of an emulsion-type carbon fiber sizing agent, can solve the problems of carbon fiber damage, high energy consumption, influence on the strength of carbon fiber, etc., and achieves the reduction of the amount of filaments, simple operation and good stability. Effect

Inactive Publication Date: 2015-12-23
UNIV OF JINAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these fiber surface treatment methods consume too much energy, and have cert

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Select the raw materials according to the weight of the weight as follows:

[0044] Epoxy resin E-44: 100;

[0045] Acetone: 10.0 copies;

[0046] EL-40: 6.5 parts;

[0047] JFC-2: 1.5 copies;

[0048] Oxide graphene: 3.0 copies;

[0049] Remove water: 150 copies.

[0050] Follow the following method to prepare oxygen graphene modified emulsion carbon fiber oxygen resin:

[0051] Place the above main slurry ring oxygen resin, emulsifier, diluent, and penetrating agent in a cup of water in a 50 ° C to cream, and mix and mix well.Use a high shear dispersing emulsifier at a constant rate of 6000rpm at the room temperature at a high speed dispersing at the room temperature. At the same time, add water to the above mixture at a rate of 2 parts / min.After 80min, get the paste emulsion.Finally, the oxygen oxygenne is poured into the above emulsion in the form of aqueous solution to obtain the carbon fibrous emulsion -type pulp -alcoholic gallery -molty carbon fiber emulsion.

Embodiment 2

[0053] Select the raw materials according to the weight of the weight as follows:

[0054] Epoxy resin E-51: 100;

[0055] Acetone: 50.0 copies;

[0056] Tween-80: 13.5 parts;

[0057] JFC-2: 4.5 parts;

[0058] Oxide graphene: 10 parts;

[0059] Remove water: 150 copies.

[0060] Follow the following method to prepare oxygen graphene modified emulsion carbon fiber oxygen resin:

[0061] Place the above main slurry ring oxygen resin, emulsifier, diluent, and penetrating agent in a cup of water in a 50 ° C to cream, and mix and mix well.Use a high shear dispersing emulsifier at a constant rate of 9000rpm at the room temperature at a high speed dispersing at the room temperature. At the same time, add water to the above mixture at a rate of 2 parts / min.After 80min, get the paste emulsion.Finally, the oxygen oxygenne is poured into the above emulsion in the form of aqueous solution to obtain the carbon fibrous emulsion -type pulp -alcoholic gallery -molty carbon fiber emulsion.

Embodiment 3

[0063] Select the raw materials according to the weight of the weight as follows:

[0064] Epoxy resin E-55: 100;

[0065] Acetone: 20 copies;

[0066] Farm milk 1601: 10 copies;

[0067] JFC-2: 2.5 parts;

[0068] Oxide graphene: 5 copies;

[0069] Remove water: 150 copies.

[0070] Follow the following method to prepare oxygen graphene modified emulsion carbon fiber oxygen resin:

[0071] Place the above main slurry ring oxygen resin, emulsifier, diluent, and penetrating agent in a cup of water in a 50 ° C to cream, and mix and mix well.Use a high shear dispersing emulsifier at a constant rate of 7000rpm at the room temperature at a high speed dispersing at the room temperature. At the same time, add water to the above mixture at a rate of 2 parts / min.After 80min, get the paste emulsion.Finally, the oxygen oxygenne is poured into the above emulsion in the form of aqueous solution to obtain the carbon fibrous emulsion -type pulp -alcoholic gallery -molty carbon fiber emulsion.

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Abstract

The invention discloses a formula and preparing method of a carbon fiber sizing agent for reinforcing polypropylene. Compared with traditional solvent type sizing agents, the prepared sizing agent has the advantages of being low in toxicity, low in cost, low in pollution and the like with water serving as the continuous phase. Besides, the sizing agent is suitable for a polypropylene resin matrix and solves the problem of poor cohesiveness between carbon fiber and polypropylene resin. When the sizing agent is used for sizing, the post processing capacity of carbon fiber is improved remarkably, the cohesiveness of the interface between carbon fiber and polypropylene matrix resin is high, and the macroscopical mechanical strength of a carbon fiber/polypropylene composite material is improved to a large extent.

Description

Technical field [0001] The invention involves a recipe and preparation method of a lotion of lactating carbon fiber slurry, which specializes in the formula and preparation method of a mitro -oxidized graphene -modified emulsion carbon fiber slurry. Background technique [0002] Carbon fiber has excellent performance of high -ratio, high ratio, high temperature resistance, and corrosion resistance. It is used as an enhanced body for composite materials and is widely used in various fields.At present, the commonly used carbon fiber resin base composite material is mainly thermosetry resin.In the past two decades, with the rapid development of industry composite materials, the application of various industries has become more and more widely used.Harmic gas volatilization and waste recycling of thermosett resin composite materials are particularly tricky.The thermoplastic resin base composite material is recycled with its available, and the molding time of the product is short and ...

Claims

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Application Information

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IPC IPC(8): C08L63/02C08L23/12C08K3/04C08J5/06D06M15/55D06M11/74
Inventor 王婷马小龙葛曷一王翠翠滕朝阳李阳
Owner UNIV OF JINAN
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