High-activity catalyst regenerative liquid and preparation method thereof, and resurrection device
A high-activity catalyst and regeneration liquid technology, applied in the direction of catalyst regeneration/reactivation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve problems such as degradation of service characteristics, inability to maintain normal operation, and end of catalyst life. The effect of enhancing the activity
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Embodiment 1
[0029] Highly active catalyst regeneration solution, including the following components by weight:
[0030]
[0031] Wherein, the regeneration preparation liquid includes sodium chloride and ethanol aqueous solution, the concentration of sodium chloride is 0.5 mol / l, and the concentration of ethanol aqueous solution is 60wt%.
[0032] The preparation method comprises the following steps:
[0033] (1) measure nitric acid and regeneration preparation solution, join nitric acid in regeneration preparation solution, mix completely, make A solution;
[0034] (2) Weigh sodium dodecylbenzene sulfonate, vinylbisstearamide and titanium dioxide respectively, first mix vinylbisstearamide and titanium dioxide completely, add to 60wt% ethanol aqueous solution and stir to dissolve, then add ten Sodium dialkylbenzene sulfonate, obtains the B solution that is equivalent to the volume of A solution;
[0035] (3) The solution A is added to the solution B by means of dropwise addition to ob...
Embodiment 2
[0037] Highly active catalyst regeneration solution, including the following components by weight:
[0038]
[0039] Wherein, the regeneration preparation liquid includes sodium sulfate and ethanol aqueous solution, the concentration of sodium sulfate is 2mol / l, and the concentration of ethanol aqueous solution is 50wt%.
[0040] The preparation method comprises the following steps:
[0041] (1) Measure sulfuric acid and regeneration preparation solution, join sulfuric acid in regeneration preparation solution, mix completely, make A solution;
[0042] (2) Take sodium lauryl sulfate, stearic acid monoglyceride and titanium dioxide respectively, first stearic acid monoglyceride and titanium dioxide are completely mixed, join in 50wt% ethanol aqueous solution and stir to dissolve, then add dodecane Sodium sulfate to prepare B solution, the volume ratio of A solution to B solution is 1~3:2;
[0043] (3) The solution A is added to the solution B by means of dropwise addition ...
Embodiment 3
[0045] Highly active catalyst regeneration solution, including the following components by weight:
[0046]
[0047] Wherein, the regeneration preparation liquid includes sodium chloride and ethanol aqueous solution, the concentration of sodium chloride is 1.5 mol / l, and the concentration of ethanol aqueous solution is 40wt%.
[0048] The preparation method comprises the following steps:
[0049] (1) Measure the hydrochloric acid and the regeneration preparation solution, add the hydrochloric acid to the regeneration preparation solution, mix completely, and prepare the A solution;
[0050] (2) Weigh polyethylene glycol, polyvinylpyrrolidone and titanium dioxide respectively, first mix polyvinylpyrrolidone and titanium dioxide completely, add to 40wt% ethanol aqueous solution and stir to dissolve, then add polyethylene glycol to prepare B solution, A The volume ratio of the solution to the B solution is 1 to 3:2;
[0051] (3) The solution A is added to the solution B by m...
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