A kind of pbt plastic and its preparation process
A preparation process and technology for plastics, applied in the field of PBT plastic and its preparation, can solve the problems of decreased mechanical properties of PBT plastics, poor safety performance, poor flame retardancy, etc., and achieve good fatigue resistance and dimensional stability, good flame retardant effect, The effect of high mechanical strength
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Embodiment 1
[0018] Mix 100kg polybutylene terephthalate (PBT), 60kg polyethylene terephthalate (PET), 25kg terephthalic acid, 13kg magnesium hydroxide, 13kg aluminum hydroxide to form a mixture M ; The mixture M and 17kg of glass fiber are mixed and sent into a twin-screw extruder for extrusion and granulation. The temperature of the extruder is controlled at 200° C., and the rotating speed of the screw is 200 rpm to obtain pellets; the pellets are baked at 230° C. Bake for 20 minutes to form a molten PBT slurry, add 2kg of dibutyltin and send it to the esterification reactor, and carry out the esterification reaction at a temperature of 260°C and a pressure of 10KPa for 20 minutes to obtain the PET esterification product N; the PET esterification product N and 5 kg of zinc sulfide were mixed and sent to an injection molding machine for injection molding. The injection molding temperature was 200° C. and the injection molding pressure was 70 MPa. After cooling, the PET plastic was obtained...
Embodiment 2
[0019] Example 2 Mix 100kg polybutylene terephthalate (PBT), 70kg polyethylene terephthalate (PET), 30kg terephthalic acid, 17kg magnesium hydroxide, and 17kg aluminum hydroxide, The mixture M is formed; the mixture M is mixed with glass fibers and sent to a twin-screw extruder for extrusion and granulation. The temperature of the extruder is controlled at 230°C, and the rotation speed of the screw is 280rpm to obtain pellets; the pellets are heated at 250°C Bake under low temperature for 40min to form a molten PBT slurry, add 3kg of stannous octoate and send it into the esterification reactor, and carry out the esterification reaction at a temperature of 300°C and a pressure of 30KPa for 35min to obtain the PET esterification product N; PET Esterification product N was mixed with 7 kg of zinc sulfide, and sent to an injection molding machine for injection molding at an injection temperature of 245° C. and an injection pressure of 85 MPa. After cooling, the PBT plastic was obta...
Embodiment 3
[0021] Mix 100kg polybutylene terephthalate (PBT), 65kg polyethylene terephthalate (PET), 27kg terephthalic acid, 15kg magnesium hydroxide, 15kg aluminum hydroxide to form a mixture M ; The mixture M and 19kg of glass fibers are mixed and sent into a twin-screw extruder for extrusion and granulation. The temperature of the extruder is controlled at 210° C., and the rotating speed of the screw is 250 rpm to obtain pellets; the pellets are baked at 240° C. Bake for 30 minutes to form a molten PBT slurry, add 2.5kg of triphenyltin and send it into the esterification reactor, and carry out the esterification reaction at a temperature of 275°C and a pressure of 15KPa for 28 minutes to obtain PET esterification product N; The PET esterification product N was mixed with 6 kg of zinc sulfide, and fed into an injection molding machine for injection molding. The injection molding temperature was 230° C., and the injection molding pressure was 77 MPa. After cooling, the PBT plastic was ob...
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Abstract
Description
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Application Information
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