A cadmium sulfide-zinc oxide core-shell multilayer nanorod array photocatalytic material and preparation method thereof
A technology of nanorod array and photocatalytic material, which is applied in the field of cadmium sulfide-zinc oxide core-shell multilayer nanorod array photocatalytic material and its preparation, can solve the problem of few surface active sites, high recombination probability of photogenerated carriers, Low utilization rate of visible light and other problems, to achieve the effect of improved photocatalytic performance, simple preparation method, and controllable loading amount
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0035] A cadmium sulfide-zinc oxide core-shell multilayer nanorod array photocatalytic material, the preparation method of which comprises the following steps:
[0036] 1) 0.75mol Zn(Ac) 2 (zinc acetate) and 0.75mol lC 2 h 7 Disperse NO (ethanolamine) in 50mL of ethylene glycol methyl ether, transfer it to a two-necked flask, pass in inert gas Ar and keep stirring, then place it in an oil bath at 60°C for 30 minutes, and transfer it to an Erlenmeyer flask after cooling to room temperature Medium aging for 24h, to get ZnO sol;
[0037] 2) The obtained ZnO sol is spin-coated onto the clean FTO glass surface by a desktop homogenizer under the condition of low speed and high speed (low speed is 600r / min, high speed is 1300r / min);
[0038] 3) Put the glass sheet evenly coated with ZnO sol in step 2) into a muffle furnace and heat it at a heating rate of 5°C / min to 300°C for 10 minutes, then cool it naturally to room temperature and take it out to obtain ZnO crystal seeds;
[00...
Embodiment 2
[0049] A cadmium sulfide-zinc oxide core-shell multilayer nanorod array photocatalytic material, the preparation method of which comprises the following steps:
[0050] 1) 0.75mol Zn(Ac) 2 (zinc acetate) and 1.5mol C 2 h 7 Disperse NO (ethanolamine) in 50mL of ethylene glycol methyl ether, transfer to a two-necked flask, pass in an inert gas Ar and keep stirring, then place it in an oil bath at 45°C for 40 minutes, and transfer it to an Erlenmeyer flask after cooling to room temperature Medium aging for 48h, to get ZnO sol;
[0051] 2) The obtained ZnO sol is spin-coated onto the clean FTO glass surface by a desktop homogenizer under the condition of low speed and high speed (low speed is 600r / min, high speed is 1300r / min);
[0052] 3) Put the glass sheet evenly coated with ZnO sol in step 2) into a muffle furnace and heat it at a heating rate of 1°C / min to 400°C for 10 minutes, then cool it naturally to room temperature and take it out to obtain ZnO crystal seeds;
[0053...
Embodiment 3
[0058] A cadmium sulfide-zinc oxide core-shell multilayer nanorod array photocatalytic material, the preparation method of which comprises the following steps:
[0059] 1) 0.75mol Zn(Ac) 2 (zinc acetate) and 0.75mol C 2 h 7 Disperse NO (ethanolamine) in 50mL of ethylene glycol methyl ether, transfer it to a two-necked flask, pass in inert gas Ar and keep stirring, then place it in an oil bath at 60°C for 30 minutes, and transfer it to an Erlenmeyer flask after cooling to room temperature Medium aging for 24h, to get ZnO sol;
[0060] 2) The obtained ZnO sol is spin-coated onto the clean FTO glass surface by a desktop homogenizer under the condition of low speed and high speed (low speed is 600r / min, high speed is 1300r / min);
[0061] 3) Put the glass sheet evenly coated with ZnO sol in step 2) into a muffle furnace and heat it at a heating rate of 5°C / min to 300°C for 10 minutes, then cool it naturally to room temperature and take it out to obtain ZnO crystal seeds;
[006...
PUM
| Property | Measurement | Unit |
|---|---|---|
| diameter | aaaaa | aaaaa |
| length | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More