Liquid organic silicon doping hexagonal boron nitride material and automatic preparation and industrial application method thereof

A technology of hexagonal boron nitride and organic silicon, which is applied in the field of optoelectronic components, can solve problems such as adhesion and sealing that are difficult to meet the requirements of use, easy yellowing and aging resistance, and achieve the effect of protecting light decay and improving thermal conductivity

Inactive Publication Date: 2016-06-15
DONG GUAN CHI MING ELECTRONICS TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Epoxy resin and polyurethane potting adhesives can achieve a good sealing effect with engineering plastic substrates, but due to the problems of easy yellowing and poor aging resistance of epoxy resin potting adhesives and polyurethane potting adhesives, they are used in In practical applications, silicone potting adhesives are widely used for potting protection of optoelectronic components due to their excellent weather resistance, aging resistance, high and low temperature resistance, mechanical and electrical insulation properties, etc.
However, engineering plastics and silicone potting adhesives are non-homogeneous materials after all, and the adhesion and sealing properties are difficult to meet higher requirements for use.

Method used

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  • Liquid organic silicon doping hexagonal boron nitride material and automatic preparation and industrial application method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] First put hexagonal boron nitride and silane coupling agent KH-570 into the mixing device at a mass ratio of 100:0.8, and after high-speed stirring for 30 minutes, surface-activated hexagonal boron nitride is obtained, and then 58.9 parts of vinyl Silicone oil, 40 parts of surface-activated hexagonal boron nitride, 0.1 part of ethynyl cyclohexanol and 1.0 part of platinum catalyst are delivered to mixer I with a stirrer through a precise metering system; 40 parts of ethylene Base silicone oil, 18 parts of hydrogen-containing silicone oil and 42 parts of surface-activated hexagonal boron nitride are transported to mixer II with a stirrer through an accurate metering and feeding system; after stirring for 10 minutes respectively, component A and component B are obtained. Components; after that, components A and B are transported 1:1 through the precise synchronous feeding system in a vacuum-tight condition, and enter the static mixing pipeline, and then enter the precision...

Embodiment 2

[0041] First put hexagonal boron nitride and silane coupling agent KH-570 into the mixing device at a mass ratio of 100:1.0, and after high-speed stirring for 30 minutes, surface-activated hexagonal boron nitride is obtained, and then 39.57 parts of vinyl Silicone oil, 60 parts of surface-activated hexagonal boron nitride, 0.03 parts of ethynyl cyclohexanol and 0.4 parts of platinum catalyst are delivered to mixer I with a stirrer through a precise metering system; 35 parts of ethylene Base silicone oil, 10 parts of hydrogen-containing silicone oil and 55 parts of surface-activated hexagonal boron nitride are transported to mixer II with a stirrer through an accurate metering and feeding system; after stirring for 10 minutes respectively, component A and component B are obtained. Components; after that, components A and B are transported 1:1 through the precise synchronous feeding system in a vacuum-tight condition, and enter the static mixing pipeline, and then enter the preci...

Embodiment 3

[0043] First put hexagonal boron nitride and silane coupling agent KH-570 into the mixing device at a mass ratio of 100:1.0, and after high-speed stirring for 30 minutes, surface-activated hexagonal boron nitride is obtained, and then 39.1 parts of vinyl Silicone oil, 60 parts of surface-activated hexagonal boron nitride, 0.08 parts of ethynyl cyclohexanol and 0.82 parts of platinum catalyst are delivered to mixer I with a stirrer through a precise metering system; 40.8 parts of ethylene Base silicone oil, 14.2 parts of hydrogen-containing silicone oil and 45 parts of surface-activated hexagonal boron nitride are transported to mixer II with a stirrer through an accurate metering system; after stirring for 10 minutes, component A and component B are obtained. Components; after that, components A and B are transported 1:1 through the precise synchronous feeding system in a vacuum-tight condition, and enter the static mixing pipeline, and then enter the precision injection system...

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Abstract

The invention discloses a liquid organic silicon-doped hexagonal boron nitride material and its automatic preparation and industrial application methods. The material is composed of component A composed of vinyl silicone oil, surface-activated hexagonal boron nitride, inhibitor and catalyst, and group B composed of vinyl silicone oil, hydrogen-containing silicone oil and surface-activated hexagonal boron nitride grouped. Its automatic preparation and industrial application method, the steps are as follows: 1) A and B components are automatically transported and mixed, and then enter the precision injection system; 2) At the same time, the silver-plated stone black ene composite metal sheet is automatically transported to the mold setting 3) Then after glue injection, curing, wrapping, slicing, chip sticking, gold wire connection, potting glue potting, it is transformed into components such as LED light source and IC patch. The liquid organic silicon-doped hexagonal boron nitride material prepared by the invention has excellent characteristics such as high and low temperature resistance, high molding efficiency, good sealing performance, and low cost, and can be widely used in various fields of optoelectronic components.

Description

technical field [0001] The invention relates to a liquid organic silicon-doped hexagonal boron nitride material and its automatic preparation and industrial application method, belonging to the technical field of photoelectric components. Background technique [0002] At present, in the field of optoelectronic components, the materials used for surface mount device (SMD) patches and lead brackets, electronic connectors, IC bases, etc. are usually high temperature resistant engineering plastics, such as polyphthalamide (PPA), poly 1,4-cyclohexanedimethanol terephthalate (PCT), etc. However, PPA has the problems of poor high and low temperature resistance and aging resistance and serious waste of secondary nozzle materials in practical applications. Although PCT materials have good temperature resistance, they also have poor bonding with silicone potting adhesives and nozzle materials cannot be recycled. defect. For components with heat dissipation requirements, a large amou...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L83/07C08L83/05C08K9/06C08K3/38C08K5/05
CPCC08L83/04C08K2201/003C08K2201/014C08L2205/025C08L2205/03C08K9/06C08K2003/385C08K5/05
Inventor 蔡明波
Owner DONG GUAN CHI MING ELECTRONICS TECH CO LTD
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