Method for preparing diamond-silicon carbide-cobalt disilicide composite interlayer of diamond coating on hard alloy
A technology of composite intermediate layer and diamond coating, which is applied in the direction of metal material coating process, coating, gaseous chemical plating, etc., can solve the problem of insufficient adhesion between CVD diamond coating and cemented carbide substrate, and cannot effectively reduce the diamond coating. The peak shear stress of the film, the inability to further reduce micro pores and other problems, achieve broad industrialization prospects, easy control of process parameters, and enhanced toughness
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[0031] Example 1
[0032] Using YG6X (WC-6%Co) cemented carbide blades sold on the domestic market as the matrix, a diamond-silicon carbide-cobalt silicide composite intermediate layer and top diamond coating are prepared on it. The specific implementation steps are as follows:
[0033] Step 1: Perform conventional pretreatment on the substrate, ultrasonically clean the cemented carbide in alcohol for 10 minutes, and then immerse it in the ratio of KOH:K 3 [Fe(CN) 6 ]: H 2 O=1:1:10 (mass ratio) solution for 10 minutes, and then immerse in the proportion of H 2 SO 4 : H 2 O 2 = 1:10 (volume ratio) solution for 1 minute to etch the cobalt on the surface of the cemented carbide.
[0034] The second step: ultrasonically pre-nucleate the cemented carbide in an alcohol suspension containing diamond micron powder and nano powder for 60 minutes, and then ultrasonically clean with alcohol for 10 minutes.
[0035] The third step: Put the pretreated cemented carbide substrate into the vacuum cham...
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