biaxially stretched laminated film
A biaxial stretching and film technology, applied in the direction of layered products, synthetic resin layered products, packaged food, etc.
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Embodiment 1
[0216] Add to a pressure-resistant reaction vessel with an inner volume of 50L equipped with a mixer, a partial condenser, a total condenser, a pressure regulator, a thermometer, a dropping tank, a pump, an aspirator, a nitrogen inlet pipe, a bottom row valve and a wire die Accurately weighed adipic acid 13000g (88.95 moles), sodium hypophosphite 0.3749g (0.0035 moles), sodium acetate 0.1944g (0.0024 moles), after fully carrying out nitrogen replacement, the reaction vessel is airtight, and the reaction vessel is kept at While stirring at 0.4 MPaG, the temperature was raised to 170°C.
[0217] After reaching 170° C., for the molten raw material in the reaction vessel, 12042 g (88.42 moles) of m-xylylenediamine stored in the dropping tank were started to be added dropwise, and the pressure in the reaction vessel was maintained at 0.4 MPaG, and the resulting While removing the condensed water to the outside of the system, the temperature inside the reaction vessel was continuous...
Embodiment 2
[0224] A laminated biaxially stretched film was obtained in the same manner as in Example 1 except that the heat setting temperature was 215° C. and the heat setting time was 10 seconds. The physical properties of the above-mentioned (1) to (8) were evaluated for the obtained biaxially stretched laminated film.
Embodiment 3
[0226] A biaxially stretched laminated film was obtained in the same manner as in Example 1 except that the heat setting time was 10 seconds. The physical properties of the aforementioned (1) to (8) were evaluated for the obtained biaxially stretched laminated film.
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Abstract
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