Water-absorbing material and its preparation method and application
A water-absorbing material and reactor technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of easily degradable temperature resistance, strong water-absorbing materials cannot withstand salt, etc., to prevent resin degradation and increase salt resistance. performance, the effect of preventing degradation
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Embodiment 1
[0033] In this embodiment, the raw material composition of the water-absorbing material and the weight percentage of each component are as follows:
[0034] Acrylic acid: 27% to 33%;
[0035] Potassium hydroxide: 17% to 21%;
[0036] Acryloylmorpholine: 1% to 2%;
[0037] Composite crosslinking agent: 1% to 2%;
[0038] Silicon dioxide: 0.2% to 0.3%;
[0039] Tackifier: 0.04% to 0.06%;
[0040] Deionized water: 41% to 54%;
[0041] Initiator: 0.1% to 0.3%;
[0042] And the mass ratio of the acrylic acid to the potassium hydroxide is 50:31.
[0043] Concrete preparation process is as follows:
[0044] First, the tackifier is prepared;
[0045] Add 300g of acrylamide to 500g of deionized water, then add 30g of AMPS, adjust the temperature to 25°C, add 5g of initiator, after the reaction is completed, granulate and dry and crush at 70°C to obtain a tackifier.
[0046] Then, figure 1 It is a schematic flow chart of the preparation method of the water-absorbing material o...
Embodiment 2
[0056] In this embodiment, the raw material composition and the weight of each component of the water-absorbing material are as follows:
[0057] Acrylic acid: 100g;
[0058] Potassium hydroxide: 62g;
[0059] Acryloylmorpholine: 5g;
[0060] Composite crosslinking agent: 5g;
[0061] Silicon dioxide: 1g;
[0062] Viscosifier: 0.2g;
[0063] Deionized water: 190g;
[0064] Initiator: 0.5g;
[0065] Specifically, the preparation process is as follows:
[0066] First, prepare a tackifier;
[0067] Add 300g of acrylamide to 500g of deionized water, then add 30g of AMPS, adjust the temperature to 25°C, add 5g of initiator, after the reaction is completed, granulate and dry and crush at 70°C to obtain a tackifier.
[0068] Then, add 100g of acrylic acid, 190g of deionized water into the reactor, and then add 62g of potassium hydroxide for neutralization reaction, then add 5g of acryloyl morpholine, 5g of composite crosslinking agent, 1g of silicon dioxide, the above-mention...
Embodiment 3
[0074] In this embodiment, the raw material composition and the weight of each component of the water-absorbing material are as follows:
[0075] Acrylic acid: 150g;
[0076] Potassium hydroxide: 93g;
[0077] Acryloylmorpholine: 7g;
[0078]Composite crosslinking agent: 7g;
[0079] Silicon dioxide: 1.5g;
[0080] Viscosifier: 0.4g;
[0081] Deionized water: 280g;
[0082] Initiator: 1g;
[0083] Specifically, the preparation process is as follows:
[0084] First, prepare a tackifier;
[0085] Add 300g of acrylamide to 500g of deionized water, then add 30g of AMPS, adjust the temperature to 25°C, add 5g of initiator, after the reaction is completed, granulate and dry and crush at 70°C to obtain a tackifier.
[0086] Then, add 150g of acrylic acid, 280g of deionized water into the reactor, then add 93g of potassium hydroxide for neutralization reaction, then add 7g of acryloyl morpholine, 7g of composite crosslinking agent, 1.5g of silicon dioxide, 0.4g of the above-p...
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