Urea-free reactive dye printing method with special mineral soil as thickener

A technology of special minerals and reactive dyes, applied in the field of textile printing, can solve problems such as the shortage of urea and sodium alginate pastes, achieve excellent printing effects, reduce printing costs, and low prices

Active Publication Date: 2016-08-24
ZHEJIANG SCI-TECH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The purpose of the present invention is to provide a kind of urea-free reactive dye printing method using special mineral soil as a paste, aiming at problems such as the need to add a large amount of urea and the shortage of sodium alginate paste for reactive dye printing, using special mineral soil as paste, in Reactive dye printing with high surface yield, sharp contours and soft touch without urea

Method used

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  • Urea-free reactive dye printing method with special mineral soil as thickener
  • Urea-free reactive dye printing method with special mineral soil as thickener
  • Urea-free reactive dye printing method with special mineral soil as thickener

Examples

Experimental program
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Effect test

Embodiment 1

[0024] A urea-free reactive dye printing method using special mineral soil as a paste, the method is as follows:

[0025] (1) Preparation of the original paste: Weigh 45g of sodium ore and dissolve it in 55mL of distilled water, stir it to a uniform and particle-free paste system, and place it overnight to fully swell and expand the paste to obtain a mass fraction of 45% sodium 100g of the original paste of chemical mineral soil, set aside;

[0026] (2) Color paste modulation:

[0027] Color paste prescription: reactive dye (K-type reactive red P-B) 1%, urea 0%, resist salt S 0.5%, sodium bicarbonate 1%, raw paste 80%, water 17.5%; total amount 100g.

[0028] Accurately weigh 1g of K-type reactive red P-B dye, and adjust it into a slurry with a small amount of distilled water (about 10 ml);

[0029] According to the color paste prescription, weigh 80g of the original paste of sodiumized ore soil with a mass fraction of 45%, add 0.5g of anti-staining salt S and 1g of sodium b...

Embodiment 2

[0033] A kind of urea-free reactive dye printing method using special mineral soil as paste, method is as follows:

[0034] (1) Preparation of raw paste: Weigh 52g of raw ore soil and dissolve it in 48mL of distilled water, stir until a uniform and particle-free paste system; place overnight to make the paste fully swell and expand, and obtain 100g of raw ore soil with a mass fraction of 52%. ,stand-by;

[0035] (2) Color paste modulation:

[0036] Color paste prescription: reactive dye (K-type reactive orange P-2R) 2%, urea 0%, resist salt S 1%, sodium bicarbonate 2%, raw paste 70%, water 25%. The total amount is 100g.

[0037] Accurately weigh 2g of K-type reactive orange P-2R dye, and adjust it into a slurry with a small amount of distilled water (about 15 milliliters);

[0038] Weigh 70g of raw ore soil paste with a mass fraction of 52% according to the color paste prescription, add 1g of anti-dyeing salt S and 2g of sodium bicarbonate in turn, stir well, then add the p...

Embodiment 3

[0042] A urea-free reactive dye printing method using special mineral soil as a paste, the method is as follows:

[0043] (1) Preparation of raw paste: Weigh 40g of sodium ore and dissolve it in 60mL of distilled water, stir until a uniform and particle-free paste system; leave it overnight to make the paste fully swell and expand, and obtain a mass fraction of 40% sodium ore 100g soil paste, set aside;

[0044] (2) Color paste modulation:

[0045] Color paste prescription: reactive dye (K-type reactive brilliant blue P-3R) 3%, urea 0%, resist salt S 1.5%, sodium bicarbonate 3%, raw paste 60%, water 32.5%.

[0046] Accurately weigh 3g of K-type reactive brilliant blue P-3R dye, and adjust it into a slurry with a small amount of distilled water (about 15 milliliters);

[0047] According to the color paste prescription, weigh 60g of the original paste of sodiumized ore soil with a mass fraction of 40%, add 1.5g of anti-staining salt S and 3g of sodium bicarbonate in turn, stir...

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Abstract

The invention discloses a urea-free reactive dye printing method with special mineral soil as a thickener. Mill base is prepared from x% of active dye, 0.5-1.5% of resist salt S, 1-3% of sodium bicarbonate, 60-80% of stock thickener and y% of water, wherein the stock thickener is prepared from, by mass, 48-58% of raw mineral soil and 35-45% of sodium modified mineral soil. The printing process includes the steps of mill base preparing, printing, drying (80 DEG C), steaming (100-102 DEG C, 10 min), water washing (by means of cold running water), soap boiling, water washing and drying, wherein the bath ratio is 1:50, the density of soap flakes is 3 g / L, the density of sodium carbonate is 2 g / L, the temperature of soap boiling is 95 DEG C, and soap boiling time is 10 min. By means of the method, printed fabric has the printing effects of high surface color yield rate, clear pattern outline and soft hand feeling. The method has the remarkable advantages that the special mineral soil thickener replaces a sodium alginate thickener, and cost is reduced; urea-free printing reduces emission of ammonia and nitrogen, and ecological environment protection is easy.

Description

technical field [0001] The invention relates to the technical field of textile printing, in particular to a urea-free reactive dye printing method using special mineral soil as a paste. Background technique [0002] Reactive dyes can be covalently bonded with cellulose fibers, the printed fabrics have high color fastness to washing, and the reactive dyes have bright color, complete color spectrum, and simple printing process, so they are widely used in the printing of cellulose fiber fabrics. [0003] Paste is an important component of printing paste, which plays a decisive role in printing effects such as the surface color yield of printed fabrics, the outline clarity of patterns and the uniformity of color yield on block surfaces. For many years, in the printing of reactive dyes, sodium alginate is the most commonly used paste, because of the evenly distributed carboxyl groups in its macromolecular structure, it can effectively repel the reactive dyes from reacting with th...

Claims

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Application Information

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IPC IPC(8): D06P1/38D06P1/673
CPCD06P1/38D06P1/6735D06P1/67383
Inventor 邵建中黄嘉敏王莉莉黄允金张向武刘今强
Owner ZHEJIANG SCI-TECH UNIV
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