Nano lithium and sodium ion battery electrode material with bubble wrap structure and preparation method thereof
A sodium ion battery and electrode material technology, applied in battery electrodes, secondary batteries, structural parts, etc., can solve the problems of unsatisfactory battery performance and poor appearance, achieve good buffering effect, improve stability, and prolong cycle life Effect
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[0088] Example 1
[0089] Bubble paper structure Sn
[0090] 0.384g K 2 SnO 3 ·3H 2 O and 0.48g urea are dissolved in 80mL deionized water-absolute ethanol mixed solution (volume ratio 5:3), the mixed solution is stirred with a magnetic stirring device for 30 minutes and then transferred to a Teflon-lined hydrothermal kettle, And keep it at 190℃ for 10h in a blast drying box, centrifuge the resulting solution to obtain white powder and dry it at 60℃ for 12h to obtain SnO 2 Precursor. SnO obtained after drying 2 0.1g precursor was dissolved in a mixed solution of 40mL deionized water and ethanol (volume ratio 3:1), 0.2g glucose was added to the solution and sonicated for 20 minutes, stirred for 1h, and then the solution was transferred to 50mL Teflon In a lined hydrothermal kettle and kept at 190°C in a blast drying box for 10 hours, brown powder was obtained by centrifugation. In order to form a carbon film, after drying, 0.2 g of the above brown powder, 0.1 g glucose and 6.7 g s...
Example Embodiment
[0107] Example 2
[0108] 0.392g(NH 4 ) 2 MoO 4 Dissolve 0.48g urea in 80mL deionized water-absolute ethanol mixed solution (volume ratio 5:3), stir the mixed solution with a magnetic stirring device for 30 minutes, then transfer it to a Teflon-lined hydrothermal kettle, and The temperature was kept at 190°C for 10h in a blast drying box, the solution obtained after the reaction was centrifuged to obtain a white powder and dried at 60°C for 12h. MoO obtained after drying 2 0.1g precursor was dissolved in a mixed solution of 40mL deionized water and ethanol (volume ratio 3:1), 0.2g glucose was added to the solution and sonicated for 20 minutes, stirred for 1h, and then the solution was transferred to 50mL Teflon In a lined hydrothermal kettle and kept at 190°C in a blast drying box for 10 hours, brown powder was obtained by centrifugation. In order to form a carbon film, after drying, 0.2 g of the above brown powder, 0.1 g glucose and 6.7 g sodium chloride were dissolved in 50 mL...
Example Embodiment
[0110] Example 3
[0111] 0.464g GeCl 4 ·H 2 O and 0.56g urea are dissolved in 80mL deionized water-absolute ethanol mixed solution (volume ratio 5:3), the mixed solution is stirred with a magnetic stirring device for 30 minutes and then transferred to a Teflon-lined hydrothermal kettle, It was kept at 190°C for 10h in a blast drying box, and the solution obtained after the reaction was centrifuged to obtain a white powder and dried at 60°C for 12h. Take the GeO obtained after drying 2 0.1g precursor was dissolved in a mixed solution of 40mL deionized water and ethanol (volume ratio 3:1), 0.2g glucose was added to the solution and sonicated for 20 minutes, stirred for 1h, and then the solution was transferred to 50mL Teflon In a lined hydrothermal kettle and kept at 190°C in a blast drying box for 10 hours, brown powder was obtained by centrifugation. In order to form a carbon film, after drying, 0.2 g of the above brown powder, 0.1 g glucose and 6.7 g sodium chloride were disso...
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