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Preparing method and application of precious cultural relic, literature and history file and calligraphy and painting protective agent

A protective agent and cultural relic technology, applied in the preparation of precious cultural relics, calligraphy and painting protective agent, and the field of cultural and historical archives, can solve problems such as affecting the environment and human health, affecting the quality of archives, and affecting the quality of archives, achieving high adhesion firm rate and protection effect. Good, low operating cost effect

Inactive Publication Date: 2016-12-07
XUZHOU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In the past, the use of chemical agents to kill insects affected the environment and human health. The batches of vacuum nitrogen-filled insecticide containers were small, and freezing technology was used to kill insects. It was necessary to move files. Some historical files are generally not suitable for moving due to their age. Affects the quality of file preservation, and drastic changes in temperature will also have a negative impact on file quality

Method used

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  • Preparing method and application of precious cultural relic, literature and history file and calligraphy and painting protective agent
  • Preparing method and application of precious cultural relic, literature and history file and calligraphy and painting protective agent
  • Preparing method and application of precious cultural relic, literature and history file and calligraphy and painting protective agent

Examples

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Effect test

Embodiment 1

[0029] Prepare a kind of precious cultural relic, literature and history archives, calligraphy and painting protective agent according to the following steps of the present invention, and by weight:

[0030] Step 1: Add 228.562 parts of desilicate water and 20.605 parts of fatty acyl monoethanolamine polyoxyethylene ether into the esterification vertical reactor, start the mixer in the esterification vertical reactor, and set the speed at 21.849rpm , start the dual-stage heating device in the esterification vertical reaction kettle, raise the temperature to 36.586°C, add 23.504 parts of methyl tetrahydrophthalic anhydride and stir evenly, carry out the enzyme-catalyzed fluorescence reaction for 13.136 minutes, add N-formaldehyde Base-N-nitroso p-toluenesulfonamide 19.511 parts, the flow rate is 12.332m 3 The chlorine gas of / min 0.21 hour; Add 22.596 parts of 4-nitrophthalimides in the esterification vertical reactor afterwards, start the two-stage heating device in the esteri...

Embodiment 2

[0038] Prepare a kind of precious cultural relic, literature and history archives, calligraphy and painting protective agent according to the following steps of the present invention, and by weight:

[0039] Step 1: Add 453.27 parts of desilicate water and 62.307 parts of fatty acyl monoethanolamine polyoxyethylene ether into the esterification vertical reactor, start the mixer in the esterification vertical reactor, and set the speed at 67.706rpm , start the dual-stage heating device in the esterification vertical reaction kettle, raise the temperature to 37.420 ° C, add 132.222 parts of methyl tetrahydrophthalic anhydride and stir evenly, and carry out the enzyme-catalyzed fluorescence reaction. After 24.825 minutes, add N- 36.484 parts of methyl-N-nitroso-p-toluenesulfonamide, the flow rate is 53.690m 3 The chlorine gas of / min 0.86 hour; Add 79.47 parts of 4-nitrophthalimides in the esterification vertical reactor afterwards, start the two-stage heating device in the ester...

Embodiment 3

[0047] Prepare a kind of precious cultural relic, literature and history archives, calligraphy and painting protective agent according to the following steps of the present invention, and by weight:

[0048] Step 1: In the esterification vertical reactor, add 228.9562 parts of desilicate water, 20.9605 parts of fatty acyl monoethanolamine polyoxyethylene ether, start the mixer in the esterification vertical reactor, and set the speed at 21.9849rpm , start the double-stage heating device in the esterification vertical reaction kettle, raise the temperature to 36.9586°C, add 23.9504 parts of methyl tetrahydrophthalic anhydride and stir evenly, carry out the enzyme-catalyzed fluorescence reaction for 13.9136 minutes, add N-methyl tetrahydrophthalic anhydride Base-N-nitroso p-toluenesulfonamide 19.9511 parts, the flow rate is 12.9332m 3 The chlorine gas of / min is 0.921 hour; Add 22.9596 parts of 4-nitrophthalimides in the esterification vertical reactor afterwards, start the two-...

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Abstract

The invention discloses a preparing method and application of a precious cultural relic, literature and history file and calligraphy and painting protective agent. The protective agent is prepared from, by weight, silicate removal water, fatty acyl monoethanolamine polyoxyethylene ether, methyl tetrahydro phthalic anhydride, N-methyl-N-nitroso para toluene sulfonamide, 4-nitro phthalimide, 1-amino-2-tectoquinone, 4-bromine-1-amination-2-sulfoacid, dimethylhydroquinone, gold nanoparticles, diphenylmethane, dimercaptosuccinic acid, 2,6-diisopropylphenylisocyanate, 2-p-benzotrifluoride-4-methyl-5-thiazole ethyl formate, methyl-1H-benzimidazole-2-base-carbamate and p-chloro-alpha-bromo-phenylacetic acid. The preparing method has the advantages that saponification of the protective agent is prevented, and elaioplast surface tension is reduced, so that the file surface protective agent can adhere more firmly; the protective agent has the advantages of being stable in chemical property, wide in application range, good in protecting effect, free of damage to files and clean in surface.

Description

technical field [0001] The invention belongs to the field of protection of books, documents, calligraphy and painting, and in particular relates to a preparation method and application of a protective agent for precious cultural relics, cultural and historical files, and calligraphy and painting. Background technique [0002] In many archives, because the storage conditions in the warehouse do not meet the constant temperature and humidity, harmful organisms are easy to breed in the archives, such as spotted beetles, black skin beetles, sweater fish, tobacco beetles, and file thieves, etc., which often occur in the form of paper The cellulose and starch binders such as straw pulp and wood pulp in quality archives are used as food materials, which directly destroy the archive entity and cause great harm. These pests are highly adaptable to the environment and can survive for a long time in harsher living environments. Take dermatomid beetles as an example, from the low tempe...

Claims

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Application Information

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IPC IPC(8): A01N59/16A01N43/52A01N43/78A01N41/06A01P1/00A01P3/00A01P7/00
CPCA01N59/16A01N41/06A01N43/52A01N43/78A01N2300/00
Inventor 梁峙梁骁
Owner XUZHOU UNIV OF TECH
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