Graphene nano layer for photoelectric degradation
A photoelectric degradation and graphene technology, applied in the field of graphene, can solve problems such as restricting degradation efficiency, achieve the effects of ensuring the generation rate, improving the effect of tight connection, and increasing the surface area
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Embodiment 1
[0031] A graphene nano-layer for photoelectric degradation, the formula is as follows: 100 parts of graphite, 10 parts of dispersant, 2 parts of modifier, 150 parts of ethanol aqueous solution, 120 parts of graphite expansion solution, 110 parts of oxidation solution, carboxylic acid modified 18 doses.
[0032] The dispersant adopts polyvinylpyrrolidone.
[0033] The modifying agent adopts nanometer calcium carbonate.
[0034] The ethanol content in the ethanol aqueous solution is 30%.
[0035] The graphite expansion liquid adopts concentrated sulfuric acid solution added with potassium peroxodisulfate and phosphorus pentoxide, and the mass ratio of potassium peroxodisulfate, phosphorus pentoxide and concentrated sulfuric acid is 1:1:3.
[0036] Described oxidation solution adopts the acetic acid aqueous solution that adds chitosan, potassium permanganate, and described chitosan is 0.2g / L, and potassium permanganate is 0.3g / L, and the acetic acid content of described acetic ...
Embodiment 2
[0050] A graphene nano-layer for photoelectric degradation, the formula is as follows: 100 parts of graphite, 15 parts of dispersant, 8 parts of modifier, 200 parts of ethanol aqueous solution, 150 parts of graphite expansion solution, 170 parts of oxidation solution, carboxylic acid modified 26 doses.
[0051] The dispersant is sodium lauryl sulfate.
[0052] The modifying agent adopts nanometer calcium carbonate.
[0053] The ethanol content in the ethanol aqueous solution is 76%.
[0054] The graphite expansion liquid adopts concentrated sulfuric acid solution added with potassium peroxodisulfate and phosphorus pentoxide, and the mass ratio of potassium peroxodisulfate, phosphorus pentoxide and concentrated sulfuric acid is 1:1.2:6.
[0055] Described oxidation solution adopts the acetic acid aqueous solution that adds chitosan, potassium permanganate, and described chitosan is 0.35g / L, and potassium permanganate is 0.55g / L, and the acetic acid content of described acetic...
Embodiment 3
[0069] A graphene nano-layer for photoelectric degradation, its formula is as follows: 100 parts of graphite, 13 parts of dispersant, 5 parts of modifier, 170 parts of ethanol aqueous solution, 150 parts of graphite expansion solution, 140 parts of oxidation solution, carboxylic acid modification 22 doses.
[0070] The dispersant adopts polyvinylpyrrolidone.
[0071] The modifying agent adopts nanometer calcium carbonate.
[0072] The ethanol content in the ethanol aqueous solution is 56%.
[0073] The graphite expansion liquid adopts concentrated sulfuric acid solution added with potassium peroxodisulfate and phosphorus pentoxide, and the mass ratio of potassium peroxodisulfate, phosphorus pentoxide and concentrated sulfuric acid is 1:1.1:5.
[0074] Described oxidation liquid adopts the acetic acid aqueous solution that adds chitosan, potassium permanganate, and described chitosan is 0.3g / L, and potassium permanganate is 0.42g / L, and the acetic acid content of described ac...
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