Preparation method of saccharose copper complex
A technology of copper complexes and sucrose, applied in the field of complexes, can solve the problems of increasing the burden on animal bodies and the environment, reducing the absorption and utilization rate, and loss of nutrients, so as to achieve repeated utilization, reduce environmental pollution, and be easy to absorb Effect
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Embodiment 1
[0042] The preparation method of sucrose copper complex comprises the steps:
[0043] Step 1. Add 25 parts by weight of sucrose to the reaction kettle, add 40 parts by weight of water to dissolve the sucrose, add aqueous sodium hydroxide solution to alkalinize, and adjust the pH of the solution to 11;
[0044] Step 2, heating the reaction kettle, keeping the temperature in the kettle at 65° C., then adding 39 parts by weight of copper chloride to carry out the complexation reaction for 1 hour, stirring continuously during the reaction process, generating a sucrose copper solution, cooling and filtering to separate, and obtaining filter residue and filtrate;
[0045] Step 3: According to the weight ratio of filtrate: 75% ethanol aqueous solution = 1:2, add 75% ethanol aqueous solution to precipitate at room temperature, the precipitation time is 1.5 hours, the precipitate is centrifugally filtered, and the obtained waste water is recycled, and the precipitate is vacuum-dried , ...
Embodiment 2
[0049] The preparation method of sucrose copper complex comprises the steps:
[0050] Step 1. Add 28 parts by weight of sucrose to the reaction kettle, add 45 parts by weight of water to dissolve the sucrose, add aqueous sodium hydroxide solution to alkalinize, and adjust the pH of the solution to 11;
[0051] Step 2: Heating the reaction kettle, keeping the temperature in the kettle at 70°C, adding 50 parts by weight of copper sulfate for complexation reaction for 1.5 hours, stirring continuously during the reaction process, generating sucrose copper solution, cooling and filtering to obtain filter residue and filtrate, press the filtrate ;
[0052] Step 3: According to the weight ratio of filtrate: 75% ethanol aqueous solution = 1:2, add 75% ethanol aqueous solution to carry out normal temperature precipitation, the precipitation time is 2 hours, the precipitate is subjected to centrifugal suction filtration, and the waste water obtained is recycled, and the precipitate is v...
Embodiment 3
[0056] The preparation method of sucrose copper complex comprises the steps:
[0057] Step 1. Add 32 parts by weight of sucrose to the reaction kettle, add 50 parts by weight of water to dissolve the sucrose, and then alkalize the solution by adding aqueous sodium hydroxide solution to adjust the pH of the solution to 12;
[0058] Step 2, heating the reaction kettle, keeping the temperature in the kettle at 75° C., then adding 50 parts by weight of copper chloride for complexation reaction for 2 hours, stirring continuously during the reaction process to generate a sucrose copper solution, cooling, filtering and separating to obtain filter residue and filtrate;
[0059] Step 3: According to the weight ratio of filtrate:75% ethanol aqueous solution=1:2, add 75% ethanol aqueous solution to carry out normal temperature precipitation, the precipitation time is 3 hours, the precipitate is subjected to centrifugal suction filtration, and the waste water obtained is recycled, and the ...
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