Preparation method of flexible transparent conductive film with super amphiphobic function
A transparent conductive film, super-amphiphobic technology, used in cable/conductor manufacturing, circuits, electrical components, etc., can solve the problems of insufficient transparency, poor adhesion of conductive coatings, and poor flexibility, and achieve high transparency. , good self-cleaning performance, good flexibility and chemical resistance
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Embodiment 1
[0047] (1) Preparation of wire-shaped silver nanowires
[0048] Dissolve silver salt, guide agent and metal salt in a solvent, heat up to 120 degrees Celsius, react for 4 hours, centrifuge, and then wash with ethanol to obtain linear silver nanowires; wherein silver salt, guide agent, metal salt And the mass ratio of solvent is 1:0.5:0.001:20;
[0049] The silver salt is silver nitrate; the solvent is ethylene glycol; the guiding agent is polyethylene glycol; the metal salt is sodium chloride;
[0050] (2) Preparation of addition type transparent silicone rubber solution
[0051] The platinum catalyst is added to the low-viscosity vinyl silicone oil, hydrogen-containing silicone oil, MQ resin and inhibitor system, and the silicone resin is obtained by stirring evenly; among them, the low-viscosity vinyl silicone oil, hydrogen-containing silicone oil, MQ resin, inhibitor and platinum The mass ratios of the catalysts are: 1:0.05:0.005:0.0001:0.0001;
[0052] Wherein, the viny...
Embodiment 2
[0067] (1) Preparation of wire-shaped silver nanowires
[0068] Dissolve silver salt, guide agent and metal salt in a solvent, heat up to 160 degrees Celsius, react for 8 hours, centrifuge, and then wash with ethanol to obtain linear silver nanowires; wherein silver salt, guide agent, metal salt And the mass ratio of the solvent is 1:5: 0.005: 50;
[0069] Wherein the silver salt is silver perchlorate; the guiding agent is polyvinyl pyrrolidone; the metal salt is potassium chloride; the solvent is propylene glycol;
[0070] (2) Preparation of addition type transparent silicone rubber solution
[0071] The platinum catalyst is added to the low-viscosity vinyl silicone resin, hydrogen-containing silicone oil, MQ resin and inhibitor system, and the silicone resin is obtained by stirring evenly; among them, the low-viscosity vinyl silicone resin, hydrogen-containing silicone oil, MQ resin, inhibitor and the mass ratio of platinum catalyst are: 1: 0.1: 0.01: 0.0002: 0.0005;
[0...
Embodiment 3
[0087] (1) Preparation of wire-shaped silver nanowires
[0088] Dissolve silver salt, guide agent and metal salt in a solvent, heat up to 140 degrees Celsius, react for 6 hours, centrifuge, and then wash with ethanol to obtain silver nanowires; wherein silver salt, guide agent, metal salt and solvent The mass ratio of 1:1:0.004:40;
[0089] Wherein the silver salt is silver fluoride; the guiding agent is polyvinylpyrrolidone; the metal salt is ammonium chloride; the solvent is polyethylene glycol;
[0090] (2) Preparation of addition type transparent silicone rubber solution
[0091] The platinum catalyst is added to the low-viscosity vinyl silicone resin, hydrogen-containing silicone oil, MQ resin and inhibitor system, and the silicone resin is obtained by stirring evenly; among them, the low-viscosity vinyl silicone resin, hydrogen-containing silicone oil, MQ resin, inhibitor And the mass ratio of platinum catalyst are: 1:0.08:0.008:0.0001:0.0001;
[0092] Wherein, the vi...
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