Gardenia yellow yeast microcapsule and preparation method thereof
The technology of gardenia yellow pigment and microcapsules is applied in the field of yeast microcapsules of gardenia yellow pigment and its preparation, which can solve the problems of expensive equipment, residual chemical reagents and the like, and achieves improved stability, easy biodegradation and good safety. Effect
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Embodiment 1
[0033] a) Take 1000 g of ripe fruits with shells of Gardenia jasminoides, pulverize them with a traditional Chinese medicine pulverizer, pass through a 40-mesh sieve, add 8 times the amount of 50% ethanol, extract at 30-70° C. for 2 hours, and filter with gauze to obtain a crude extract of gardenia yellow pigment;
[0034] b) The crude extract containing gardenia yellow pigment in step a) is micro-filtered with a 200nm ceramic membrane at 30°C and a pressure of 0.2MPa until clarified; then with a 3000Da ultrafiltration membrane at room temperature and a pressure of 0.4MPa Refined by ultrafiltration; then use a nanofiltration membrane with a molecular weight cut-off of 150Da to concentrate by nanofiltration at room temperature and an operating pressure of 3.0MPa; freeze-dry the concentrated solution to obtain a freeze-dried powder of gardenia yellow pigment; During the process, when the remaining feed liquid is 30% of the weight of the raw material liquid, water of 1 times the a...
Embodiment 2
[0039] a) Take 1000 g of ripe fruits with shells of Gardenia jasminoides, pulverize them with a traditional Chinese medicine grinder, pass through a 40-mesh sieve, add 5 times the amount of 45% ethanol, extract at 30-70° C. for 2 hours, and filter with gauze to obtain a crude extract of gardenia yellow pigment;
[0040] b) The crude extract containing gardenia yellow pigment in step a) is micro-filtered with a 200nm ceramic membrane at 30°C and a pressure of 0.2MPa until clarified; then with a 3000Da ultrafiltration membrane at room temperature and a pressure of 0.4MPa Refined by ultrafiltration; then use a nanofiltration membrane with a molecular weight cut-off of 150Da to concentrate by nanofiltration at room temperature and an operating pressure of 3.0MPa; freeze-dry the concentrated solution to obtain a freeze-dried powder of gardenia yellow pigment; During the process, when the remaining feed liquid is 30% of the weight of the raw material liquid, water of 1 times the amou...
Embodiment 3
[0045] a) Take 1000 g of ripe fruits with shells of Gardenia jasminoides, pulverize them with a traditional Chinese medicine grinder, pass through a 40-mesh sieve, add 8 times the amount of 50% ethanol, extract at 30-70° C. for 2 hours, and filter with gauze to obtain a crude extract of gardenia yellow pigment;
[0046] b) The crude extract containing gardenia yellow pigment in step a) is microfiltered with a 150nm ceramic membrane at 40°C and a pressure of 0.2MPa until it becomes clear; Refined by ultrafiltration; then use a nanofiltration membrane with a molecular weight cut-off of 100Da to concentrate by nanofiltration at room temperature and an operating pressure of 3.0MPa; freeze-dry the concentrated solution to obtain a freeze-dried powder of gardenia yellow pigment; During the process, when the remaining feed liquid is 30% of the weight of the raw material liquid, water of 1 times the amount of the remaining feed liquid can be added to continue microfiltration, and repea...
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