Propolis-type plant antibacterial mouth wash and preparation method thereof
A plant antibacterial and mouthwash technology, applied in the field of mouthwash, can solve the problems of drug-resistant people's oral cavity, tooth discoloration, and single effect, and achieve the effects of low preparation cost, good protection, and simple and easy operation
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Embodiment 1
[0047] A preparation method of supercritical propolis extract:
[0048] Select 100g of high-quality propolis, freeze it at -18°C for 48 hours, then crush the propolis, put it into a high-pressure supercritical extraction device, pass in CO2, add 20g of 60% ethanol as an entrainer, and set the extraction temperature and pressure to 60°C and 20Mpa , the separation temperature and pressure are 50°C, 5.5Mpa, CO 2 The flow rate is 10L / h. After static extraction for 50 minutes, then dynamic extraction for 2 hours, the extracted product was collected, and concentrated under reduced pressure at 45°C until there was no solvent to obtain 10 g of supercritical propolis extract.
[0049] A preparation method of Chinese herbal medicine extract:
[0050] Mix 100g of the six kinds of mixtures of ebony, rhizoma rhizome, gallnut, locust tree, almond, and duckbill flower in a mass ratio of 3:1:2:2:1:1 and grind them to 200 mesh, add 500g of 50% ethanol After soaking the solution for 2 hours...
Embodiment 2
[0059] The difference between the present invention and embodiment 1 is: a kind of propolis type plant antibacterial mouthwash, is made up of the component of following mass parts:
[0060] Supercritical propolis extract 2%, Chinese herbal medicine extract 25%, essential oil mixture 0.35%, edible ethanol 18%, multivitamin 6%, deionized water balance.
Embodiment 3
[0062] The difference between the present invention and embodiment 1 is: a kind of propolis type plant antibacterial mouthwash, is made up of the component of following mass parts:
[0063] Supercritical propolis extract 5%, Chinese herbal medicine extract 23%, essential oil mixture 0.5%, edible ethanol 15%, multivitamin 7%, deionized water balance.
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