Material applied to the field of OLED

A field, coupling reaction technology, applied in the field of OLED

Active Publication Date: 2017-03-08
EVERDISPLAY OPTRONICS (SHANGHAI) CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In fact, although the scope of OLED applications continues to expand, there are still deficiencies, and one of the basic factors that determine the performance of OLEDs is the material problem. The deficiency is the focus of OLED research work

Method used

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  • Material applied to the field of OLED
  • Material applied to the field of OLED
  • Material applied to the field of OLED

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] 1. A compound used in the field of OLEDs, the structure of which is shown in formula (I-1):

[0041]

[0042] 2, the preparation method of described compound comprises:

[0043] Add the toluene of 0.1mol intermediate A-1, 0.1mol intermediate B-1 and 1000mL in the reaction bottle, add potassium carbonate 200mmol and 1mmol catalyst Pd[P(C 6 h 5 ) 3 ] 4 , reflux reaction under nitrogen protection for 24 hours, after the completion of the reaction, add 500ml of distilled water, cool and filter, extract with dichloromethane, wash with salt water, separate the organic layer, remove the organic solvent by rotary evaporation, pass the crude product through the column, and then use dichloromethane and Compound (I-1) was obtained by ethanol recrystallization and purification;

[0044] in,

[0045] 3. Molecular weight characterization MS 639.2311

[0046] H-NMR: 7.53(2H), 7.62(4H), 7.71(4H), 7.58(1H), 7.67(1H), 7.76(1H), 7.34(2H), 7.49(2H), 7.64(2H), 7.61 (2H), 7.64(2H...

Embodiment 2

[0048] 1. A compound used in the field of OLEDs, the structure of which is shown in formula (I-2):

[0049]

[0050] 2, the preparation method of described compound comprises:

[0051] In reaction bottle, add the toluene of 0.1mol intermediate A-2, 0.1mol intermediate B-2 and 1000mL, add potassium carbonate 200mmol and 1mmol catalyst Pd[P(C 6 h 5 ) 3 ] 4 , reflux reaction under nitrogen protection for 24 hours, after the completion of the reaction, add 500ml of distilled water, cool and filter, extract with dichloromethane, wash with salt water, separate the organic layer, remove the organic solvent by rotary evaporation, pass the crude product through the column, and then use dichloromethane and Compound (I-2) was obtained by ethanol recrystallization and purification;

[0052] in,

[0053] 3. Molecular weight characterization MS 655.2082

[0054] H-NMR: 7.53(2H), 7.62(4H), 7.71(4H), 7.58(1H), 7.75(1H), 7.78(1H), 7.39(2H), 7.49(2H), 7.64(2H), 7.61 (2H), 7.64(2H), ...

Embodiment 3

[0056] 1. A compound used in the field of OLEDs, the structure of which is shown in formula (I-3):

[0057]

[0058] 2, the preparation method of described compound comprises:

[0059] In reaction bottle, add the toluene of 0.1mol intermediate A-3, 0.1mol intermediate B-3 and 1000mL, add potassium carbonate 200mmol and 1mmol catalyst Pd[P(C 6 h 5 ) 3 ] 4 , reflux reaction under nitrogen protection for 24 hours, after the completion of the reaction, add 500ml of distilled water, cool and filter, extract with dichloromethane, wash with salt water, separate the organic layer, remove the organic solvent by rotary evaporation, pass the crude product through the column, and then use dichloromethane and Compound (I-3) was obtained by ethanol recrystallization and purification;

[0060] in,

[0061] 3. Molecular weight characterization MS 655.2082

[0062] H-NMR: 7.53(2H), 7.62(4H), 7.71(4H), 7.58(1H), 7.67(1H), 7.76(1H), 7.34(2H), 7.49(2H), 7.62(2H), 7.67 (2H), 7.56(2H), ...

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PUM

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Abstract

The invention provides a material applied to the field of OLED. The material is characterized by comprising a compound having the general structure shown in the formula (I) which is defined in the description, wherein R is an aromatic compound; -A is defined in the description and X is O or S. The compound disclosed by the invention can be applied to a hole transmission layer, a light-emitting layer and an electron transport layer in the OLED device, and the OLED device with better performance is finally obtained.

Description

technical field [0001] The invention relates to the field of OLEDs, in particular to a material used in the field of OLEDs. Background technique [0002] As a display screen, TFT-LCD is a non-self-illuminating display. The light must be projected through the backlight, and then penetrate the polarizer, glass substrate, liquid crystal layer, color filter, Glass substrates, polarizers and other related components finally enter the human eye for imaging to achieve the display function. In practical applications, TFT-LCD display screens have disadvantages such as slow response rate, power consumption, and narrow viewing angle, which are not enough to be a perfect display screen. [0003] OLED, as a new display technology, has the characteristics of self-luminescence, and is prepared by using a very thin organic material coating and a glass substrate. These organic materials emit light when an electric current is passed through them. At present, the basic structure of an OLED ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D405/10C07D409/10C09K11/06H01L51/54
CPCC09K11/06C07D405/10C07D409/10C09K2211/1059C09K2211/1044C09K2211/1007C09K2211/1011C09K2211/1088C09K2211/1092H10K85/654H10K85/6574H10K85/6576H10K85/6572H10K50/11
Inventor 杨红领
Owner EVERDISPLAY OPTRONICS (SHANGHAI) CO LTD
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