MnP2O7 microcrystalline opacified matt glaze material composition having photocatalysis function and preparation method thereof
A matte glaze and composition technology, applied in the field of ceramic glaze, can solve the problems of no photocatalytic function glaze report, no photocatalytic material application report, etc., and achieve good crystal decoration effect and good opacity effect. , the effect of smooth glaze
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[0029] The present invention adopts simple preparation method, can prepare the MnP that can be widely used on the surface of traditional ceramics such as building sanitation and daily-use ceramics 2 o 7 Microcrystalline opacified matte glaze composition. The photocatalytic function MnP provided by the present invention is exemplarily illustrated below 2 o 7 The preparation method of the microcrystalline opacified matte glaze composition.
[0030] Using quartz, potassium feldspar, spodumene, sodium phosphate, MnO, lithium carbonate, etc. as raw materials, according to the following mass chemical composition ratio SiO 2 :Al 2 o 3 :P 2 o 5 :MnO:Li 2 O: Na 2 O:K 2O=(12-14):(4-6):(47-49):(1.5-2.5):(12-14):(6-8):(11-13) for batching.
[0031] Dry mix and grind the raw materials of the above powder A, and pass through a 40-60 sieve to obtain a mixture. Then put it into a crucible, put it into an electric furnace and keep it warm at 1300°C-1340°C for 35-45min. The powder ...
Embodiment 1
[0039] Example 1: MnP 2 o 7 The mass percentage is 5% photocatalytic functional ceramic opacity glaze
[0040] 1) First, mix quartz, potassium feldspar, spodumene, sodium phosphate, MnO, and lithium carbonate raw materials according to the following mass chemical composition ratios. SiO 2 :Al 2 o 3 :P 2 o 5 :MnO:Li 2 O: Na 2 O:K 2 O=13:5:48:2:13:7:12;
[0041] 2) Dry mix and grind the above powders, pass through 40 sieves to obtain the mixture, put it into a crucible, put it into an electric furnace at 1320°C for 40 minutes, take it out and pour it into water to quench to make a frit. Take the frit out of the water, put it into a ball mill after drying, and grind it finely. The ratio of control material (frit): ball: water is 1:1:0.8. After grinding for 3 hours, pass through a 250-mesh sieve, and dry for later use. The powder is recorded as material A;
[0042] 3) MnO and NaH 2 PO 4 Powder according to mass ratio MnO: NaH 2 PO 4 : KF=1:3.6:0.12 Dry mix evenly, ...
Embodiment 2
[0046] Example 2: MnP 2 o 7 The mass percentage is 6% photocatalytic functional ceramic opacity glaze
[0047] 1) First, mix quartz, potassium feldspar, spodumene, sodium phosphate, MnO, and lithium carbonate raw materials according to the following mass chemical composition ratios. SiO 2 :Al 2 o 3 :P 2 o 5 :MnO:Li 2 O: Na 2 O:K 2 O=12:4:49:2.5:13.5:8:13;
[0048] 2) Dry mix and grind the above powders, pass through 60 sieves to obtain the mixture, put it into a crucible, put it into an electric furnace at 1300°C for 35 minutes, take it out and pour it into water to quench to make a frit. Take the frit out of the water, put it into a ball mill after drying, and grind it finely. The ratio of control material (frit): ball: water is 1:1:0.8, pass through a 250-mesh sieve after grinding for 2-4 hours, and dry for later use . The powder is recorded as material A;
[0049] 3) MnO and NaH 2 PO 4 Powder according to mass ratio MnO: NaH 2 PO 4 : KF=1:3.4:0.1 Dry mix ev...
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