Preparation method of catalytically active ceramic wool for flue gas denitrification
A technology of catalytic activity and ceramic wool, which is applied in the field of catalytic active ceramic wool for flue gas denitrification, can solve the problems of reducing convenience and achieve the effect of simple installation, good catalytic activity and improved activity
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Embodiment 1
[0021] A method for preparing catalytically active ceramic wool for flue gas denitrification, the preparation process comprising the following steps:
[0022] (1) Prepare a mixed solution containing catalytically active components; wherein, based on the total weight of the mixture solution, zirconium nitrate is 39wt%, manganese nitrate is 28wt%, ferric nitrate is 12wt%, and cerium nitrate is 21wt%; Triton X -100 (octylphenyl polyoxyethylene ether) 0.3%wt%.
[0023] (2) Immerse the zirconia ceramic fiber cotton in the solution prepared in step (1); wherein, the immersion time is 3min, the solution temperature is 45°C; the fiber diameter of the zirconia ceramic fiber cotton is 3μm, and the bulk density is 95kg / m 3 .
[0024] (3) After removing excess solution from the fiber cotton impregnated with the solution in step (2), place the fiber cotton in a closed container filled with ammonia gas for fumigation; the time is 30 minutes.
[0025] (4) Microwave-dry the fiber cotton fum...
Embodiment 2
[0029] A method for preparing catalytically active ceramic wool for flue gas denitrification, the preparation process comprising the following steps:
[0030] (1) preparation contains the mixed solution of catalytically active component; Wherein, based on the total weight of the mixture solution, zirconium nitrate 42wt%, manganese nitrate is 26wt%, ferric nitrate is 8wt%, cerium nitrate is 24wt%; Triton X-100 (octylphenyl polyoxyethylene ether) 0.5%wt%.
[0031] (2) Immerse the zirconia ceramic fiber cotton in the solution prepared in step (1); wherein, the immersion time is 5min, and the solution temperature is 50°C; the fiber diameter of the zirconia ceramic fiber cotton is 5 μm, and the bulk density is 103 kg / m 3 .
[0032] (3) After the fiber cotton impregnated with the solution in step (2) is removed with a dryer to remove excess solution, place the fiber cotton in a closed container filled with ammonia gas for fumigation; the time is 45 minutes.
[0033] (4) Microwave-...
Embodiment 3
[0037] A method for preparing catalytically active ceramic wool for flue gas denitrification, the preparation process comprising the following steps:
[0038] (1) Prepare a mixed solution containing catalytically active components; wherein, based on the total weight of the mixture solution, zirconium nitrate is 36wt%, manganese nitrate is 24 wt%, ferric nitrate is 15wt%, and cerium nitrate is 25 wt%; Triton X -100 (octylphenyl polyoxyethylene ether) 0.6%wt%.
[0039] (2) Immerse zirconia ceramic fiber cotton in the solution prepared in step (1); wherein, the immersion time is 8 minutes, and the solution temperature is 55°C; the fiber diameter of zirconia ceramic fiber cotton is 5 μm, and the bulk density is 103 kg / m 3 .
[0040] (3) After removing excess solution from the fiber cotton impregnated in step (2) with a drier, place the fiber cotton in a closed container filled with ammonia gas for fumigation; the time is 50 minutes.
[0041] (4) Microwave-dry the fiber cotton fu...
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