Nano-crystalline anisotropic magnet prepared by 3D (three-dimensional) printing technique

A 3D printing and anisotropic technology, applied in the direction of magnetic objects, magnetic materials, inorganic materials, etc., to achieve the effects of shortening the production cycle, improving production efficiency, and high magnetic properties of magnets

Inactive Publication Date: 2017-05-17
解伟
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The existing technology requires corresponding molds to prepare magnets, and it takes a certain amount of time and cost to make molds. After the product is demoulded, subsequent processing is required, and there is a certain processing cost.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Step (1), smelting NdFeB into an alloy;

[0021] In step (2), the magnetic powder of irregular shape is made after the strip and jet mill, the strip speed is 15m / s, and the counter-jet jet mill is adopted, the air pressure of the nozzle is 0.3MPa, and the classifying wheel speed is 3000rpm;

[0022] Step (3), using low temperature, surfactant-assisted external magnetic field high-energy ball milling technology to produce 10nm nano-magnetic powder of the above powder;

[0023] In step (4), the irregular-shaped magnetic powder is spray-dried to obtain a spherical magnetic powder. The obtained spherical magnetic powder has a particle size of 40 μm, and the spherical magnetic powder has good fluidity and can be used for 3D printing;

[0024] In step (5), the spherical magnetic powder is uniformly mixed with a binder and a processing aid, the binder is epoxy resin or phenolic resin, and the processing aid includes a lubricant and a plasticizer; wherein the spherical magnetic...

Embodiment 2

[0030] Step (1), melting manganese and bismuth into an alloy;

[0031] In step (2), the magnetic powder of irregular shape is made after stripping and jet milling, the speed of stripping is 20m / s, and the counter-jet jet mill is adopted, the air pressure of the nozzle is 1MPa, and the speed of classifying wheel is 3000rpm;

[0032] Step (3), using low temperature, surfactant-assisted external magnetic field high-energy ball milling technology to produce 50nm nano-magnetic powder of the above powder;

[0033] In step (4), the manganese bismuth nano magnetic powder is uniformly mixed with a binding agent and a processing aid, the binding agent is nylon, and the processing aid includes a lubricant and a plasticizer; wherein the spherical magnetic powder is 90%, and the binding agent The agent is 9%, the processing aid is 1%, and the above percentages are volume percentages;

[0034] In step (5), the mixed powder is sent into an extruder, and the temperature of the extruder is 25...

Embodiment 3

[0039] Step (1), melting samarium cobalt into an alloy;

[0040] Step (2), make irregularly shaped magnetic powder after stripping and jet milling, the speed of stripping is 25m / s, using a counter-jet jet mill, the air pressure of the nozzle is 0.6MPa, and the classifying wheel speed is 3000rpm;

[0041] Step (3), using low temperature, surfactant-assisted external magnetic field high-energy ball milling technology to produce 20nm nano-magnetic powder of the above powder;

[0042] In step (4), the irregular-shaped magnetic powder is obtained by atomic atomization method to obtain spherical magnetic powder, the obtained spherical magnetic powder has a particle size of 45 μm, and the spherical magnetic powder has good fluidity and can be used for 3D printing;

[0043] In step (5), the spherical magnetic powder is uniformly mixed with a binding agent and a processing aid, the binding agent is nylon, and the processing aid includes a lubricant and a plasticizer; wherein the spheri...

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Abstract

The invention discloses a method for preparing a nano-crystalline anisotropic magnet by a 3D (three-dimensional) printing technique. The method includes that: hard magnetic alloys including neodymium iron boron alloy, samarium cobalt alloy, aluminum nickel cobalt alloy, manganese bismuth alloy, samarium iron alloy and the like are melted; the alloys are prepared into irregularly-shaped magnetic powder through melt-spinning and airflow grinding; the irregularly-shaped magnetic powder is subjected to spray drying and the like so as to obtain spherical nanometer agglomerated powder; the spherical nanometer agglomerated powder is mixed with a binding agent and a processing agent uniformly; the mixture is conveyed into a hot extruding machine and extruded to form silks; a three-dimensional model is established by computer software according to the size and the shape of a product, and the product model is subjected to layered slicing; the three-dimensional model is lead into a 3D printer; the silks are conveyed into 3D printer and heated to soften, through an extruder and a movable spraying nozzle with a heating function, the material is extruded and deposited on a workbench which can be heated, and the extruded material is solidified on the workbench, accumulated and adhered layer by layer and magnetized during printing until the product is printed completely. The method for preparing the nano-crystalline anisotropic magnet by the 3D printing technique has the advantages that the prepared product is high in cost performance and processing performance, production period of the magnet can be shorted, and production cost of the magnet can be reduced.

Description

technical field [0001] The invention relates to a permanent magnetic alloy, in particular to a magnet for 3D printing, in particular to a method for preparing an anisotropic nanocrystalline magnet using 3D printing technology. Background technique [0002] One of the key technologies of 3D printing lies in the morphology and properties of the materials used. The printing material is generally a spherical powder, and the spheroidization rate of the powder is generally required to be greater than 98%. Only a high spheroidization rate can ensure that the printing powder is evenly and smoothly transported to the printing pool, so as to obtain a printed product with a dense structure and a low defect rate. At present, it is difficult to prepare high-end fine-grained spherical metal powder in China, and this powder depends on imports. [0003] Using low temperature, surfactant-assisted external magnetic field high-energy ball milling technology to prepare single-domain nano-magn...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F41/02H01F1/057H01F1/08B22F3/00B22F10/00
CPCH01F1/0578H01F41/0273B22F3/00
Inventor 不公告发明人
Owner 解伟
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