Lithium sulfide solid electrolyte material containing silver iodide and silver bromide and preparation method of lithium sulfide solid electrolyte material
A solid electrolyte, silver bromide technology, applied in solid electrolytes, electrolyte battery manufacturing, non-aqueous electrolytes, etc., can solve the problems of low battery coulombic efficiency, hinder lithium ion passing, difficult to maintain charge-discharge cycle, etc., to improve ion conduction. rate, and the effect of improving ion conductivity
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Embodiment 1
[0029] 1) Sulfide preparation mixing process:
[0030] By mass percent, take by weighing 40% lithium sulfide and 60% phosphorus sulfide in the glove box with argon atmosphere protection of low moisture (≤1ppm), low oxygen content (≤1ppm), and mix with zirconium dioxide After the balls are matched, they are sealed into a ball mill jar, and the mass ratio of the zirconia balls in the jar to the mixture is 2:0.7; the sealed ball mill jars are packed in a planetary high-energy ball mill and pre-mixed by a dry ball mill, and the milling time is After 5 hours, a ternary mixture of lithium sulfur and phosphorus (LiPS mixture for short) was obtained;
[0031] 2) Second high energy ball milling process:
[0032] In a glove box protected by an argon atmosphere with low moisture (≤1ppm) and low oxygen content (≤1ppm) with safe lights (such as red light), silver iodide powder (particle size) equivalent to 2.5% of the above LiPS mixture mass 200-250 mesh) and silver bromide powder (grain...
Embodiment 2
[0040] Repeat Example 1, the difference is:
[0041] In step 1), the mass percentages of lithium sulfide and phosphorus sulfide are 50% and 50% respectively, and the ball milling time is 10 hours.
[0042] After pressing the solid electrolyte powder prepared in this example into a standard sample, the ion conductivity of the sample in this example was measured to be 6.0×10 at a room temperature of 25° C. -4 S / cm.
Embodiment 3
[0044] Repeat Example 1, the difference is:
[0045] In step 1), the mass percentages of lithium sulfide and phosphorus sulfide are respectively 50% and 50%, and the time of ball milling is 2 hours;
[0046] In step 2), the silver iodide and silver bromide powders have a particle size of 200-250 mesh, the silver iodide powder is added in an amount equivalent to 3.5% of the LiPS mixture mass, and the silver bromide powder added in an amount equivalent to 2.5% of the LiPS mixture mass;
[0047] After the solid electrolyte powder prepared in this example was pressed into a standard sample, the ion conductivity of the sample in this example was measured at 25°C at room temperature by using the CHI660 electrochemical workstation by AC impedance method to be 6.2×10 -4 S / cm.
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