A kind of preparation method of near ultraviolet LED with composite electron blocking layer
An electron blocking layer, near-ultraviolet technology, applied in circuits, electrical components, nanotechnology for materials and surface science, etc., can solve problems such as low light efficiency, improve luminous efficiency, relieve compressive stress, and improve holes extended effect
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[0024] A preparation method of a near-ultraviolet LED with a composite electron blocking layer, comprising the following steps:
[0025] S1, the Al 2 o 3The substrate is treated in a hydrogen atmosphere with a reaction chamber pressure of 100 torr at 1080°C-1100°C for 5-10 minutes, and then the temperature and pressure are reduced to keep the temperature at 530°C-550°C, and the reaction chamber pressure is 500torr. Under a hydrogen atmosphere, The V / III molar ratio is 500-1300, and a low-temperature GaN buffer layer with a thickness of 20-30 nanometers is three-dimensionally grown.
[0026] S2, keeping the temperature at 1000-1500° C., the reaction chamber pressure at 200-300 torr, and the V / III molar ratio at 1000-1300 in a hydrogen atmosphere, growing a high-temperature u-GaN layer with a thickness of 1-3 microns.
[0027] S3, keep the temperature at 1000-1500°C, the pressure of the reaction chamber is 100-200torr, under the hydrogen atmosphere, the V / III molar ratio is 10...
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