Solar positive silver paste with high aspect ratio and preparation method thereof
A high aspect ratio, solar energy technology, applied in the direction of cable/conductor manufacturing, conductive materials dispersed in non-conductive inorganic materials, electrical components, etc., to achieve the effect of increasing aspect ratio, improving rheology, and improving conversion efficiency
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Embodiment 1
[0036] A method for preparing a solar front silver paste with a high aspect ratio, comprising the steps of:
[0037] (1) Preparation of organic phase carrier
[0038] 4.7 parts of N-type ethylcellulose with 45% ethoxylate content, 8.7 parts of T-type ethylcellulose with 50% ethoxylate content, 13.3 parts of tributyl phosphate, 13.3 parts of dipentaerythritol ester, hydrogenated castor oil 13.3 parts, Tween 20:10 parts, 36.7 parts of diethylene glycol butyl ether acetate, after mixing evenly, heated and stirred at 45°C for 30 minutes to make a uniform and transparent solution, that is, to prepare an organic phase carrier;
[0039] (2) Preparation of glass paste
[0040] Take 3 parts of glass powder with a D50 of 0.6 μm and a Tg point of 262 °C, and 15 parts of the organic phase carrier prepared in step (1), disperse evenly on a disperser, and roll on a three-roll machine to a fineness below 5um to obtain a glass slurry;
[0041] (3) Preparation of silver paste
[0042] Take...
Embodiment 2
[0045] A method for preparing a solar front silver paste with a high aspect ratio, comprising the steps of:
[0046] (1) Preparation of organic phase carrier
[0047] 4.2 parts of N-type ethyl cellulose with 45% ethoxy content, 4.2 parts of T-type ethyl cellulose with 50% ethoxy content, 4.2 parts of dibutyl phthalate, 12.5 parts of dipentaerythritol ester, 1.7 parts of polyamide-modified hydrogenated castor oil, Tween 80:8.3 parts, and 64.9 parts of terpineol were mixed evenly, and heated and stirred at 50°C for 40 minutes to make a uniform and transparent solution, which was formulated as an organic phase carrier;
[0048] (2) Preparation of glass paste
[0049] Take 3 parts of glass powder with a D50 of 0.9 μm and a Tg point of 439 ° C, and 12 parts of the organic phase carrier prepared in step (1), and disperse evenly on the disperser, and then roll it on a three-roller machine until the fineness is below 5um to obtain glass slurry;
[0050] (3) Preparation of silver pa...
Embodiment 3
[0054] A method for preparing a solar front silver paste with a high aspect ratio, comprising the steps of:
[0055] (1) Preparation of organic phase carrier
[0056] 8 parts of N-type ethyl cellulose with an ethoxy content of 45%, 11.4 parts of dioctyl adipate, 17 parts of tributyl phosphate, 5.7 parts of fumed silica, Tween 80: 5.7 parts, mixed two After mixing 52.2 parts of dibasic acid ester (DBE) evenly, heat and stir at 65°C for 20 minutes to make a uniform and transparent solution, that is, to prepare an organic phase carrier;
[0057] (2) Preparation of glass paste
[0058] Take 1.2 parts of glass powder with a D50 of 2.0 μm and a Tg point of 340 ° C, and 8.8 parts of the organic phase carrier prepared in step (1) are uniformly dispersed on the disperser, and then rolled on a three-roll machine to a fineness of 5 μm or less to obtain a glass slurry;
[0059] (3) Preparation of silver paste
[0060] Take 90 parts of silver powder with a D50 of 1.2 μm and a tap densi...
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