A kind of cowhide processing method
A processing method and technology of cowhide, applied in leather surface treatment, tanning treatment, small raw hide/large raw hide/leather/fur treatment, etc., can solve the problems of low molecular weight, inability to improve leather elasticity, etc., and achieve the effect of improving elasticity
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Embodiment 1
[0033] This embodiment provides a polyurethane finishing agent S1, its preparation method and a cowhide treatment method using the polyurethane finishing agent.
[0034] The preparation method of described polyurethane finishing agent S1 comprises the following steps:
[0035] S11: A reactant composed of 0.1mol of polyoxypropylene triol (abbreviated as PPG) with a functionality of Fn=3 and a number average molecular weight of Mn=1000g / mol and 0.3mol of isophorone diisocyanate (abbreviated as IPDI) And the dibutyltin dilaurate (English abbreviation DBTDL) catalyst of 20ppm joins in the there-necked flask of a 1000ml;
[0036] S12: Under the condition of an 85°C oil bath, mechanically stir the reactants in the three-necked flask. After 2 hours of reaction, the polyurethane prepolymer formed by the reaction is cooled to room temperature. The schematic diagram of the chemical reaction is as follows figure 2 As shown, the PPG and IPDI in the polyurethane prepolymer are cross-link...
Embodiment 2
[0061] This embodiment provides a polyurethane finishing agent S2, its preparation method and a cowhide treatment method using the polyurethane finishing agent.
[0062] The preparation method of described polyurethane finishing agent S2 comprises the following steps:
[0063] S21: Reactant composed of 0.1 mol of polyoxyethylene ether triol with functionality Fn=3, number average molecular weight Mn=4000g / mol, 0.3 mol of cyclohexane dimethyl diisocyanate and 50 ppm of dibutyltin dilaurate Catalyst joins in the there-necked flask of a 1000ml;
[0064] S22: Under the condition of an oil bath at 90°C, mechanically stir the reactants in the three-necked flask, and after 3 hours of reaction, cool down the polyurethane prepolymer formed by the reaction to room temperature, and the polymer in the polyurethane prepolymer Oxyethylene ether triol and cyclohexane dimethyl diisocyanate crosslinked;
[0065] S23: using ethanol to dilute the polyurethane prepolymer to a solution with a cu...
Embodiment 3
[0082] This embodiment provides a polyurethane finishing agent S3, its preparation method and a cowhide treatment method using the polyurethane finishing agent.
[0083] The preparation method of described polyurethane finishing agent S3 comprises the following steps:
[0084] S31: A reactant composed of 0.1 mol of polyoxypropylene diol (abbreviated as PEG) and 0.2 mol of toluene diisocyanate (abbreviated as TDI) with number average molecular weight Mn=8000g / mol and 100ppm The dibutyltin dilaurate catalyst joins in a 1000ml there-necked flask;
[0085] S32: Under the condition of an oil bath at 90°C, mechanically stir the reactants in the three-necked flask, and after 4 hours of reaction, cool down the polyurethane prepolymer formed by the reaction to room temperature, and the PEG in the polyurethane prepolymer and TDI cross-connect;
[0086] S33: using isopropanol to dilute the polyurethane prepolymer to a solution with a curing amount of 50%;
[0087] S34: Adding 0.3 mol ...
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